# 1 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc"
;t1ir_l1.mv    transposed as is by BRC
;avance-version (07/04/03)
;Adapted for high Q probes and H2O samples.  M> Voehler, 3/2012
;T1 measurement using inversion recovery and water suppression using 1-1 pulse sequence

; Typcial paramerters for this measurement:  relaxation delay 15 to 20 sec
; 16 to 24 variable dealys between 1 msec and 5 sec; 120 us binomial dealy at 500 MHz
; these experiments took about 3 hr when aquiring 4 ds, 32 aquisiton scans and 16 delay times
; on an approximately 100 uM DNA sample.

;$CLASS=HighRes
;$DIM=2D
;$TYPE=
;$SUBTYPE=
;$COMMENT=
# 17 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc"
prosol relations=<triple>
# 1 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Avance.incl" 1
;Avance3.incl
;   for AV III
;
;avance-version (13/06/17)
;
;$CLASS=HighRes Incl
;$COMMENT=


# 169 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Avance.incl"
;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $
# 18 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc" 2

# 1 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Delay.incl" 1
;Delay.incl  -  include file for commonly used delays
;
;version (13/08/07)
;
;$CLASS=HighRes Incl
;$COMMENT=

# 9 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Delay.incl"
;general delays

define delay DELTA
define delay DELTA1
define delay DELTA2
define delay DELTA3
define delay DELTA4
define delay DELTA5
define delay DELTA6
define delay DELTA7
define delay DELTA8
define delay DELTA9
define delay DELTA10
define delay DELTA11
define delay DELTA12
define delay DELTA13
define delay DELTA14
define delay DELTA15
define delay DELTA16

define delay TAU
define delay TAU1
define delay TAU2
define delay TAU3
define delay TAU4
define delay TAU5
define delay TAU6
define delay TAU7
define delay TAU8
define delay TAU9
# 40 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Delay.incl"
define delay INCR1
define delay INCR2
define delay INCR3
define delay INCR4
define delay INCR5
define delay INCR6


;delays for centering pulses
# 50 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Delay.incl"
define delay CEN_HN1
define delay CEN_HN2
define delay CEN_HN3
define delay CEN_HC1
define delay CEN_HC2
define delay CEN_HC3
define delay CEN_HC4
define delay CEN_HP1
define delay CEN_HP2
define delay CEN_CN1
define delay CEN_CN2
define delay CEN_CN3
define delay CEN_CN4
define delay CEN_CP1
define delay CEN_CP2


;loop counters
# 69 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Delay.incl"
define loopcounter COUNTER
define loopcounter SCALEF
define loopcounter FACTOR1
define loopcounter FACTOR2
define loopcounter FACTOR3
define loopcounter FACTOR4
define loopcounter FACTOR5
define loopcounter FACTOR6


# 80 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Delay.incl"
;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $
# 19 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc" 2

# 1 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Grad.incl" 1
;Grad2.incl  -  include file for Gradient Spectroscopy
;   for TCU3
;
;avance-version (07/01/17)
;
;$CLASS=HighRes Incl
;$COMMENT=

# 27 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Grad.incl"
define list<gradient> EA=<EA>


# 31 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/Grad.incl"
;$Id: Grad2.incl,v 1.14 2012/01/31 17:49:21 ber Exp $
# 20 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc" 2


"p2=p1*2"
"d11=30m"
"acqt0=-p1*2/3.1416"
# 1 "mc_line 26 file /opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc dc-measurement inserted automatically"

    dccorr
# 26 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc"
# 26 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc"
1 ze
2 d1 pl1:f1
  p2 ph1
  vd
  p1 ph2
  4u setnmr3|0 setnmr0|34|32|33 ctrlgrad 0
  4u
  p16:gp3
  d16
  p1 ph4
  d19
  p1 ph5
  4u
  p16:gp3
  d16
  4u setnmr3^0 setnmr0^34^32^33 ctrlgrad 7
 
  go=2 ph31
  d1 wr #0 if #0 ivd
  lo to 1 times td1 
exit

ph1 = 0 0 2 2 1 1 3 3
ph2 = 0 0 2 2 1 1 3 3
ph4 = 0 0 2 2 1 1 3 3
ph5 = 2 2 0 0 3 3 1 1
ph31 = 0 0 2 2 1 1 3 3 

# 55 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc"
;pl1 : f1 channel - power level for pulse (default)
;p1 : f1 channel -  90 degree high power pulse
;p2 : f1 channel - 180 degree high power pulse
;p16 : gradient pulse  [1 msec]
;d1 : relaxation delay; 1-5 * T1
;d11 : delay for disk I/O   [30 msec]
;d16 : gradient recovery delay [ 200 usec ]
;d19 : binominal delay [115 usec]
;vd : variable delay, taken from vd-list
;ns : 8 * n
;ds : 4
;td1 : number of experiments = number of dealys in vd-list
;FnMODE : Undefined
;define VDLIST
;
;this pulse program produces a ser-file (PARMOD = 2D)
;Phase first FID then use split2D to create 1D spectra
;
;for z-only gradients :
;gpz1 : 40%  (24 G/cm)
;use gradient files:
;gpnam3 : SMSQ10.100


# 80 "/opt/topspin3.6.0/exp/stan/nmr/lists/pp/user/t1ir_l1.mv.brc"
;$Id: zg2d,v 1.6.8.1 2012/01/31 17:56:41 ber Exp $
