data_50080 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; Backbone 1H, 13C and 15N resonance assignment of USP7 TRAF-like domain free and in complex with DNA polymerase iota ; _BMRB_accession_number 50080 _BMRB_flat_file_name bmr50080.str _Entry_type original _Submission_date 2019-10-24 _Accession_date 2019-10-24 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details . loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Valles Gabrielle J. . 2 Bezsonova Irina . . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count assigned_chemical_shifts 2 spectral_peak_list 5 stop_ loop_ _Data_type _Data_type_count "1H chemical shifts" 228 "13C chemical shifts" 335 "15N chemical shifts" 228 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2020-11-08 original BMRB . stop_ loop_ _Related_BMRB_accession_number _Relationship 6939 'Backbone chemical shift assignment of USP7 in complex with EBNA1 peptide' bmrbig5 'Time-domain and peaklist datasets' stop_ _Original_release_date 2019-12-02 save_ ############################# # Citation for this entry # ############################# save_citations_1 _Saveframe_category entry_citation _Citation_full . _Citation_title ; Backbone 1H, 13C and 15N resonance assignment of USP7 TRAF-like domain free and in complex with DNA polymerase iota ; _Citation_status 'in preparation' _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code . _PubMed_ID ? loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Ashton Nicholas W. . 2 Valles Gabrielle J. . 3 Bezsonova Irina . . 4 Woodgate Roger . . stop_ _Journal_abbreviation 'to be published' _Journal_volume . _Journal_issue . _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first . _Page_last . _Year . _Details . save_ ################################## # Molecular system description # ################################## save_assembly_1 _Saveframe_category molecular_system _Mol_system_name 'USP7 TRAF-like domain' _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label 'USP7 TRAF-like domain' $entity_1 stop_ _System_molecular_weight . _System_physical_state native _System_oligomer_state ? _System_paramagnetic no _System_thiol_state . _Database_query_date . _Details . save_ ######################## # Monomeric polymers # ######################## save_entity_1 _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class protein _Name_common entity_1 _Molecular_mass . _Mol_thiol_state 'all free' _Details ; Full protein sequence: 1 MET 2 ASN 3 HIS 4 GLN 5 GLN 6 GLN 7 GLN 8 GLN 9 GLN 10 GLN 11 LYS 12 ALA 13 GLY 14 GLU 15 GLN 16 GLN 17 LEU 18 SER 19 GLU 20 PRO 21 GLU 22 ASP 23 MET 24 GLU 25 MET 26 GLU 27 ALA 28 GLY 29 ASP 30 THR 31 ASP 32 ASP 33 PRO 34 PRO 35 ARG 36 ILE 37 THR 38 GLN 39 ASN 40 PRO 41 VAL 42 ILE 43 ASN 44 GLY 45 ASN 46 VAL 47 ALA 48 LEU 49 SER 50 ASP 51 GLY 52 HIS 53 ASN 54 THR 55 ALA 56 GLU 57 GLU 58 ASP 59 MET 60 GLU 61 GLY 62 ASP 63 THR 64 SER 65 TRP 66 ARG 67 SER 68 GLU 69 ALA 70 THR 71 PHE 72 GLN 73 PHE 74 THR 75 VAL 76 GLU 77 ARG 78 PHE 79 SER 80 ARG 81 LEU 82 SER 83 GLU 84 SER 85 VAL 86 LEU 87 SER 88 PRO 89 PRO 90 CYS 91 PHE 92 VAL 93 ARG 94 ASN 95 LEU 96 PRO 97 TRP 98 LYS 99 ILE 100 MET 101 VAL 102 MET 103 PRO 104 ARG 105 PHE 106 TYR 107 PRO 108 ASP 109 ARG 110 PRO 111 HIS 112 GLN 113 LYS 114 SER 115 VAL 116 GLY 117 PHE 118 PHE 119 LEU 120 GLN 121 CYS 122 ASN 123 ALA 124 GLU 125 SER 126 ASP 127 SER 128 THR 129 SER 130 TRP 131 SER 132 CYS 133 HIS 134 ALA 135 GLN 136 ALA 137 VAL 138 LEU 139 LYS 140 ILE 141 ILE 142 ASN 143 TYR 144 ARG 145 ASP 146 ASP 147 GLU 148 LYS 149 SER 150 PHE 151 SER 152 ARG 153 ARG 154 ILE 155 SER 156 HIS 157 LEU 158 PHE 159 PHE 160 HIS 161 LYS 162 GLU 163 ASN 164 ASP 165 TRP 166 GLY 167 PHE 168 SER 169 ASN 170 PHE 171 MET 172 ALA 173 TRP 174 SER 175 GLU 176 VAL 177 THR 178 ASP 179 PRO 180 GLU 181 LYS 182 GLY 183 PHE 184 ILE 185 ASP 186 ASP 187 ASP 188 LYS 189 VAL 190 THR 191 PHE 192 GLU 193 VAL 194 PHE 195 VAL 196 GLN 197 ALA 198 ASP 199 ALA 200 PRO 201 HIS 202 GLY 203 VAL 204 ALA 205 TRP ; ############################## # Polymer residue sequence # ############################## _Residue_count 145 _Mol_residue_sequence ; GDTSWRSEATFQFTVERFSR LSESVLSPPCFVRNLPWKIM VMPRFYPDRPHQKSVGFFLQ CNAESDSTSWSCHAQAVLKI INYRDDEKSFSRRISHLFFH KENDWGFSNFMAWSEVTDPE KGFIDDDKVTFEVFVQADAP HGVAW ; loop_ _Residue_seq_code _Residue_author_seq_code _Residue_label 1 61 GLY 2 62 ASP 3 63 THR 4 64 SER 5 65 TRP 6 66 ARG 7 67 SER 8 68 GLU 9 69 ALA 10 70 THR 11 71 PHE 12 72 GLN 13 73 PHE 14 74 THR 15 75 VAL 16 76 GLU 17 77 ARG 18 78 PHE 19 79 SER 20 80 ARG 21 81 LEU 22 82 SER 23 83 GLU 24 84 SER 25 85 VAL 26 86 LEU 27 87 SER 28 88 PRO 29 89 PRO 30 90 CYS 31 91 PHE 32 92 VAL 33 93 ARG 34 94 ASN 35 95 LEU 36 96 PRO 37 97 TRP 38 98 LYS 39 99 ILE 40 100 MET 41 101 VAL 42 102 MET 43 103 PRO 44 104 ARG 45 105 PHE 46 106 TYR 47 107 PRO 48 108 ASP 49 109 ARG 50 110 PRO 51 111 HIS 52 112 GLN 53 113 LYS 54 114 SER 55 115 VAL 56 116 GLY 57 117 PHE 58 118 PHE 59 119 LEU 60 120 GLN 61 121 CYS 62 122 ASN 63 123 ALA 64 124 GLU 65 125 SER 66 126 ASP 67 127 SER 68 128 THR 69 129 SER 70 130 TRP 71 131 SER 72 132 CYS 73 133 HIS 74 134 ALA 75 135 GLN 76 136 ALA 77 137 VAL 78 138 LEU 79 139 LYS 80 140 ILE 81 141 ILE 82 142 ASN 83 143 TYR 84 144 ARG 85 145 ASP 86 146 ASP 87 147 GLU 88 148 LYS 89 149 SER 90 150 PHE 91 151 SER 92 152 ARG 93 153 ARG 94 154 ILE 95 155 SER 96 156 HIS 97 157 LEU 98 158 PHE 99 159 PHE 100 160 HIS 101 161 LYS 102 162 GLU 103 163 ASN 104 164 ASP 105 165 TRP 106 166 GLY 107 167 PHE 108 168 SER 109 169 ASN 110 170 PHE 111 171 MET 112 172 ALA 113 173 TRP 114 174 SER 115 175 GLU 116 176 VAL 117 177 THR 118 178 ASP 119 179 PRO 120 180 GLU 121 181 LYS 122 182 GLY 123 183 PHE 124 184 ILE 125 185 ASP 126 186 ASP 127 187 ASP 128 188 LYS 129 189 VAL 130 190 THR 131 191 PHE 132 192 GLU 133 193 VAL 134 194 PHE 135 195 VAL 136 196 GLN 137 197 ALA 138 198 ASP 139 199 ALA 140 200 PRO 141 201 HIS 142 202 GLY 143 203 VAL 144 204 ALA 145 205 TRP stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date . save_ #################### # Natural source # #################### save_natural_source_1 _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species $entity_1 Human 9606 Eukaryota Metazoa Homo sapiens stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_type _Vector_name $entity_1 'recombinant technology' . Escherichia coli . plasmid pet-28b stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Saveframe_category sample _Sample_type solution _Details ; Double labeled USP7 TRAF-like domain free; 0.9 mM 15N/13C TRAF in 20 mM phosphate buffer, pH 7.5, 250 mM NaCl, 10 mM DTT and 10% D2O (v/v). ; loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $entity_1 0.9 mM '[U-100% 13C; U-100% 15N]' 'sodium phosphate' 20 mM 'natural abundance' 'sodium chloride' 250 mM 'natural abundance' DTT 10 mM 'natural abundance' D2O 10 '% v/v' '[U-100% 2H]' stop_ save_ save_sample_2 _Saveframe_category sample _Sample_type solution _Details '15N USP7 TRAF-like domain free; 0.250 mM 15N TRAF in 20 mM phosphate buffer, pH 7.5, 250 mM NaCl, 10 mM DTT and 10% D2O (v/v).' loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $entity_1 0.250 mM '[U-100% 15N]' 'sodium phosphate' 20 mM 'natural abundance' 'sodium chloride' 250 mM 'natural abundance' DTT 10 mM 'natural abundance' D2O 10 '% v/v' '[U-100% 2H]' 'DNA polymerase iota peptide 573-584' 1.25 mM 'natural abundance' stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Saveframe_category software _Name NMRPipe _Version . loop_ _Vendor _Address _Electronic_address 'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax' . . stop_ loop_ _Task processing stop_ _Details . save_ save_software_2 _Saveframe_category software _Name NMRbox _Version . loop_ _Vendor _Address _Electronic_address 'UConn Health Center' . . stop_ loop_ _Task 'data analysis' stop_ _Details . save_ save_software_3 _Saveframe_category software _Name SPARKY _Version . loop_ _Vendor _Address _Electronic_address Goddard . . stop_ loop_ _Task 'chemical shift assignment' 'data analysis' 'peak picking' stop_ _Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Agilent _Model INOVA _Field_strength 500 _Details 'Agilent VNMRS spectrometer 500 MHz' save_ save_NMR_spectrometer_2 _Saveframe_category NMR_spectrometer _Manufacturer Agilent _Model INOVA _Field_strength 800 _Details 'Agilent VNMRS spectrometer 800 MHz' save_ ############################# # NMR applied experiments # ############################# save_2D_1H-15N_HSQC_1 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-15N HSQC' _Sample_label $sample_2 save_ save_3D_HNCA_2 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HNCA' _Sample_label $sample_1 save_ save_3D_HNCACB_3 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HNCACB' _Sample_label $sample_1 save_ save_3D_HNCO_4 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HNCO' _Sample_label $sample_1 save_ save_2D_1H-15N_HSQC_5 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-15N HSQC' _Sample_label $sample_1 save_ save_2D_1H-1H_NOESY_6 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-1H NOESY' _Sample_label $sample_2 save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units 'ionic strength' 0.250 . M pH 7.5 . pH pressure 1 . atm temperature 303 . K stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Saveframe_category chemical_shift_reference _Details 'double labeled USP7 TRAF-like domain' loop_ _Mol_common_name _Atom_type _Atom_isotope_number _Atom_group _Chem_shift_units _Chem_shift_value _Reference_method _Reference_type _External_reference_sample_geometry _External_reference_location _External_reference_axis _Indirect_shift_ratio water C 13 protons ppm 4.725 internal indirect . . . 0.251449453 water H 1 protons ppm 4.725 internal indirect . . . 1 water N 15 protons ppm 4.725 internal indirect . . . 0.101329 stop_ save_ save_chem_shift_reference_2 _Saveframe_category chemical_shift_reference _Details '15N USP7 TRAF-like domain' loop_ _Mol_common_name _Atom_type _Atom_isotope_number _Atom_group _Chem_shift_units _Chem_shift_value _Reference_method _Reference_type _External_reference_sample_geometry _External_reference_location _External_reference_axis _Indirect_shift_ratio water H 1 protons ppm 4.725 internal indirect . . . 1 water N 15 protons ppm 4.725 internal indirect . . . 0.101329 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Saveframe_category assigned_chemical_shifts _Details 'double labeled USP7 TRAF-like domain' loop_ _Experiment_label '3D HNCA' '3D HNCACB' '3D HNCO' '2D 1H-15N HSQC' '2D 1H-1H NOESY' stop_ loop_ _Sample_label $sample_1 $sample_2 stop_ _Sample_conditions_label $sample_conditions_1 _Chem_shift_reference_set_label $chem_shift_reference_1 _Mol_system_component_name 'USP7 TRAF-like domain' _Text_data_format . _Text_data . loop_ _Atom_shift_assign_ID _Residue_author_seq_code _Residue_seq_code _Residue_label _Atom_name _Atom_type _Chem_shift_value _Chem_shift_value_error _Chem_shift_ambiguity_code 1 65 5 TRP C C 175.457 0.00 . 2 65 5 TRP CA C 56.680 0.00 . 3 66 6 ARG H H 7.545 0.00 . 4 66 6 ARG C C 174.657 0.00 . 5 66 6 ARG CA C 56.150 0.04 . 6 66 6 ARG CB C 31.107 0.00 . 7 66 6 ARG N N 121.316 0.02 . 8 67 7 SER H H 8.834 0.01 . 9 67 7 SER C C 172.584 0.00 . 10 67 7 SER CA C 59.540 0.02 . 11 67 7 SER CB C 64.496 0.02 . 12 67 7 SER N N 116.502 0.06 . 13 68 8 GLU H H 7.474 0.00 . 14 68 8 GLU C C 174.742 0.00 . 15 68 8 GLU CA C 53.772 0.09 . 16 68 8 GLU CB C 33.742 0.00 . 17 68 8 GLU N N 116.283 0.03 . 18 69 9 ALA H H 8.334 0.00 . 19 69 9 ALA C C 175.147 0.00 . 20 69 9 ALA CA C 52.832 0.07 . 21 69 9 ALA CB C 23.810 0.05 . 22 69 9 ALA N N 119.026 0.01 . 23 70 10 THR H H 8.265 0.00 . 24 70 10 THR C C 174.204 0.00 . 25 70 10 THR CA C 61.633 0.02 . 26 70 10 THR CB C 70.097 0.01 . 27 70 10 THR N N 115.639 0.02 . 28 71 11 PHE H H 9.441 0.00 . 29 71 11 PHE C C 172.140 0.00 . 30 71 11 PHE CA C 55.968 0.01 . 31 71 11 PHE CB C 41.316 0.01 . 32 71 11 PHE N N 124.667 0.05 . 33 72 12 GLN H H 8.567 0.00 . 34 72 12 GLN C C 175.616 0.00 . 35 72 12 GLN CA C 53.889 0.07 . 36 72 12 GLN CB C 33.219 0.03 . 37 72 12 GLN N N 116.812 0.01 . 38 73 13 PHE H H 9.511 0.00 . 39 73 13 PHE C C 173.413 0.00 . 40 73 13 PHE CA C 55.667 0.09 . 41 73 13 PHE CB C 43.926 0.00 . 42 73 13 PHE N N 121.636 0.06 . 43 74 14 THR H H 8.778 0.00 . 44 74 14 THR C C 172.679 0.00 . 45 74 14 THR CA C 62.215 0.05 . 46 74 14 THR CB C 69.959 0.03 . 47 74 14 THR N N 126.855 0.01 . 48 75 15 VAL H H 9.110 0.01 . 49 75 15 VAL C C 174.812 0.00 . 50 75 15 VAL CA C 62.157 0.06 . 51 75 15 VAL CB C 33.123 0.11 . 52 75 15 VAL N N 129.475 0.05 . 53 76 16 GLU H H 8.105 0.00 . 54 76 16 GLU C C 175.218 0.00 . 55 76 16 GLU CA C 55.553 0.06 . 56 76 16 GLU CB C 31.181 0.12 . 57 76 16 GLU N N 125.135 0.02 . 58 77 17 ARG H H 8.900 0.00 . 59 77 17 ARG C C 178.734 0.00 . 60 77 17 ARG CA C 56.475 0.01 . 61 77 17 ARG CB C 27.934 0.02 . 62 77 17 ARG N N 118.975 0.01 . 63 78 18 PHE H H 9.250 0.00 . 64 78 18 PHE C C 177.369 0.00 . 65 78 18 PHE CA C 63.427 0.01 . 66 78 18 PHE CB C 40.058 0.00 . 67 78 18 PHE N N 121.810 0.02 . 68 79 19 SER H H 9.533 0.00 . 69 79 19 SER C C 176.512 0.00 . 70 79 19 SER CA C 61.875 0.02 . 71 79 19 SER N N 110.008 0.02 . 72 80 20 ARG H H 7.811 0.00 . 73 80 20 ARG C C 176.271 0.00 . 74 80 20 ARG CA C 54.800 0.03 . 75 80 20 ARG CB C 30.309 0.00 . 76 80 20 ARG N N 120.608 0.04 . 77 81 21 LEU H H 7.929 0.00 . 78 81 21 LEU CA C 57.532 0.00 . 79 81 21 LEU CB C 43.024 0.00 . 80 81 21 LEU N N 124.506 0.05 . 81 82 22 SER C C 173.099 0.00 . 82 82 22 SER CA C 58.037 0.05 . 83 82 22 SER CB C 65.017 0.00 . 84 83 23 GLU H H 7.693 0.01 . 85 83 23 GLU C C 173.420 0.00 . 86 83 23 GLU CA C 54.672 0.04 . 87 83 23 GLU CB C 32.300 0.04 . 88 83 23 GLU N N 120.098 0.05 . 89 84 24 SER H H 8.109 0.00 . 90 84 24 SER C C 174.646 0.00 . 91 84 24 SER CA C 58.192 0.10 . 92 84 24 SER CB C 64.627 0.11 . 93 84 24 SER N N 111.738 0.03 . 94 85 25 VAL H H 9.177 0.01 . 95 85 25 VAL C C 173.232 0.00 . 96 85 25 VAL CA C 60.307 0.10 . 97 85 25 VAL CB C 35.636 0.10 . 98 85 25 VAL N N 120.153 0.08 . 99 86 26 LEU H H 8.087 0.00 . 100 86 26 LEU C C 176.605 0.00 . 101 86 26 LEU CA C 52.998 0.04 . 102 86 26 LEU CB C 46.496 0.02 . 103 86 26 LEU N N 123.253 0.04 . 104 87 27 SER H H 8.548 0.00 . 105 87 27 SER CA C 57.344 0.06 . 106 87 27 SER CB C 63.370 0.00 . 107 87 27 SER N N 119.268 0.03 . 108 89 29 PRO C C 175.345 0.00 . 109 89 29 PRO CA C 62.320 0.00 . 110 89 29 PRO CB C 32.658 0.00 . 111 90 30 CYS H H 8.963 0.01 . 112 90 30 CYS C C 174.696 0.00 . 113 90 30 CYS CA C 57.061 0.00 . 114 90 30 CYS CB C 27.236 0.03 . 115 90 30 CYS N N 123.138 0.02 . 116 91 31 PHE H H 8.966 0.00 . 117 91 31 PHE C C 175.426 0.00 . 118 91 31 PHE CA C 58.551 0.00 . 119 91 31 PHE CB C 40.144 0.05 . 120 91 31 PHE N N 128.512 0.02 . 121 92 32 VAL H H 8.600 0.00 . 122 92 32 VAL C C 177.126 0.00 . 123 92 32 VAL CA C 63.042 0.03 . 124 92 32 VAL CB C 34.826 0.00 . 125 92 32 VAL N N 123.414 0.03 . 126 93 33 ARG H H 9.304 0.00 . 127 93 33 ARG C C 173.712 0.00 . 128 93 33 ARG CA C 56.860 0.05 . 129 93 33 ARG CB C 27.345 0.12 . 130 93 33 ARG N N 124.349 0.02 . 131 94 34 ASN H H 8.726 0.00 . 132 94 34 ASN C C 173.055 0.00 . 133 94 34 ASN CA C 54.400 0.03 . 134 94 34 ASN CB C 38.173 0.03 . 135 94 34 ASN N N 109.422 0.06 . 136 95 35 LEU H H 7.749 0.00 . 137 95 35 LEU CA C 51.327 0.02 . 138 95 35 LEU CB C 44.169 0.00 . 139 95 35 LEU N N 118.693 0.04 . 140 96 36 PRO C C 175.461 0.00 . 141 96 36 PRO CA C 61.544 0.00 . 142 96 36 PRO CB C 31.570 0.00 . 143 97 37 TRP H H 8.516 0.01 . 144 97 37 TRP C C 175.597 0.00 . 145 97 37 TRP CA C 55.234 0.04 . 146 97 37 TRP CB C 29.742 0.05 . 147 97 37 TRP N N 126.563 0.04 . 148 98 38 LYS H H 9.209 0.00 . 149 98 38 LYS C C 175.661 0.00 . 150 98 38 LYS CA C 55.018 0.05 . 151 98 38 LYS CB C 38.742 0.00 . 152 98 38 LYS N N 117.287 0.05 . 153 99 39 ILE H H 8.536 0.00 . 154 99 39 ILE C C 173.441 0.00 . 155 99 39 ILE CA C 61.948 0.07 . 156 99 39 ILE CB C 41.377 0.00 . 157 99 39 ILE N N 122.425 0.04 . 158 100 40 MET H H 9.092 0.01 . 159 100 40 MET C C 174.104 0.00 . 160 100 40 MET CA C 54.357 0.00 . 161 100 40 MET CB C 37.315 0.00 . 162 100 40 MET N N 128.295 0.07 . 163 101 41 VAL H H 8.669 0.00 . 164 101 41 VAL CA C 60.171 0.01 . 165 101 41 VAL CB C 35.758 0.00 . 166 101 41 VAL N N 125.933 0.05 . 167 102 42 MET H H 8.635 0.00 . 168 102 42 MET CA C 53.473 0.04 . 169 102 42 MET N N 120.910 0.04 . 170 107 47 PRO C C 177.062 0.00 . 171 107 47 PRO CA C 64.918 0.00 . 172 108 48 ASP H H 8.696 0.00 . 173 108 48 ASP C C 174.172 0.00 . 174 108 48 ASP CA C 54.294 0.00 . 175 108 48 ASP CB C 40.221 0.00 . 176 108 48 ASP N N 113.412 0.05 . 177 109 49 ARG H H 7.506 0.01 . 178 109 49 ARG CA C 56.666 0.03 . 179 109 49 ARG CB C 29.426 0.00 . 180 109 49 ARG N N 118.816 0.09 . 181 114 54 SER C C 172.368 0.00 . 182 114 54 SER CA C 57.680 0.09 . 183 114 54 SER CB C 67.860 0.00 . 184 115 55 VAL H H 8.971 0.01 . 185 115 55 VAL C C 173.373 0.00 . 186 115 55 VAL CA C 62.011 0.05 . 187 115 55 VAL CB C 33.897 0.00 . 188 115 55 VAL N N 119.879 0.02 . 189 116 56 GLY H H 9.379 0.00 . 190 116 56 GLY C C 170.565 0.00 . 191 116 56 GLY CA C 45.355 0.10 . 192 116 56 GLY N N 117.840 0.06 . 193 117 57 PHE H H 7.256 0.00 . 194 117 57 PHE C C 172.849 0.00 . 195 117 57 PHE CA C 55.734 0.26 . 196 117 57 PHE N N 127.670 0.02 . 197 118 58 PHE H H 9.742 0.00 . 198 118 58 PHE C C 172.554 0.00 . 199 118 58 PHE CA C 55.911 0.06 . 200 118 58 PHE CB C 43.413 0.00 . 201 118 58 PHE N N 124.417 0.04 . 202 119 59 LEU H H 9.136 0.01 . 203 119 59 LEU C C 174.078 0.00 . 204 119 59 LEU CA C 53.351 0.08 . 205 119 59 LEU N N 122.909 0.02 . 206 120 60 GLN H H 9.760 0.01 . 207 120 60 GLN C C 174.227 0.00 . 208 120 60 GLN CA C 54.151 0.03 . 209 120 60 GLN N N 127.113 0.03 . 210 121 61 CYS H H 9.434 0.01 . 211 121 61 CYS C C 173.937 0.00 . 212 121 61 CYS CA C 56.481 0.10 . 213 121 61 CYS N N 128.234 0.09 . 214 122 62 ASN H H 8.073 0.00 . 215 122 62 ASN C C 175.859 0.00 . 216 122 62 ASN CA C 53.310 0.04 . 217 122 62 ASN CB C 39.071 0.00 . 218 122 62 ASN N N 121.963 0.05 . 219 123 63 ALA H H 7.462 0.00 . 220 123 63 ALA C C 178.253 0.00 . 221 123 63 ALA CA C 54.660 0.12 . 222 123 63 ALA CB C 19.627 0.10 . 223 123 63 ALA N N 118.193 0.01 . 224 124 64 GLU H H 8.170 0.00 . 225 124 64 GLU C C 176.190 0.00 . 226 124 64 GLU CA C 56.560 0.19 . 227 124 64 GLU CB C 29.416 0.13 . 228 124 64 GLU N N 115.175 0.02 . 229 125 65 SER H H 6.800 0.00 . 230 125 65 SER C C 174.001 0.00 . 231 125 65 SER CA C 57.681 0.00 . 232 125 65 SER CB C 63.651 0.00 . 233 125 65 SER N N 112.496 0.03 . 234 126 66 ASP H H 8.750 0.01 . 235 126 66 ASP C C 176.262 0.00 . 236 126 66 ASP CA C 53.933 0.11 . 237 126 66 ASP CB C 40.605 0.01 . 238 126 66 ASP N N 125.995 0.02 . 239 127 67 SER H H 8.263 0.00 . 240 127 67 SER CA C 57.671 0.01 . 241 127 67 SER CB C 63.442 0.00 . 242 127 67 SER N N 114.767 0.02 . 243 128 68 THR C C 175.773 0.00 . 244 129 69 SER H H 8.425 0.00 . 245 129 69 SER C C 174.138 0.00 . 246 129 69 SER CA C 58.625 0.08 . 247 129 69 SER CB C 64.774 0.05 . 248 129 69 SER N N 115.640 0.01 . 249 130 70 TRP H H 6.958 0.00 . 250 130 70 TRP C C 175.299 0.00 . 251 130 70 TRP CA C 55.110 0.04 . 252 130 70 TRP CB C 30.590 0.03 . 253 130 70 TRP N N 120.690 0.03 . 254 131 71 SER H H 8.947 0.01 . 255 131 71 SER C C 174.042 0.00 . 256 131 71 SER CA C 58.966 0.06 . 257 131 71 SER CB C 65.442 0.15 . 258 131 71 SER N N 111.661 0.02 . 259 132 72 CYS H H 9.517 0.00 . 260 132 72 CYS C C 173.356 0.00 . 261 132 72 CYS CA C 60.309 0.02 . 262 132 72 CYS CB C 30.272 0.00 . 263 132 72 CYS N N 120.980 0.02 . 264 133 73 HIS H H 9.448 0.01 . 265 133 73 HIS C C 173.562 0.00 . 266 133 73 HIS CA C 57.514 0.01 . 267 133 73 HIS CB C 30.988 0.00 . 268 133 73 HIS N N 133.078 0.04 . 269 134 74 ALA H H 8.598 0.00 . 270 134 74 ALA C C 175.150 0.00 . 271 134 74 ALA CA C 51.482 0.08 . 272 134 74 ALA CB C 24.416 0.02 . 273 134 74 ALA N N 127.150 0.06 . 274 135 75 GLN H H 8.309 0.00 . 275 135 75 GLN C C 174.291 0.00 . 276 135 75 GLN CA C 54.046 0.09 . 277 135 75 GLN CB C 32.044 0.02 . 278 135 75 GLN N N 117.105 0.02 . 279 136 76 ALA H H 8.929 0.01 . 280 136 76 ALA C C 175.667 0.00 . 281 136 76 ALA CA C 50.701 0.08 . 282 136 76 ALA CB C 23.855 0.04 . 283 136 76 ALA N N 122.273 0.04 . 284 137 77 VAL H H 9.101 0.00 . 285 137 77 VAL C C 174.343 0.00 . 286 137 77 VAL CA C 62.442 0.03 . 287 137 77 VAL CB C 33.977 0.01 . 288 137 77 VAL N N 120.996 0.02 . 289 138 78 LEU H H 9.049 0.00 . 290 138 78 LEU C C 174.242 0.00 . 291 138 78 LEU CA C 55.304 0.07 . 292 138 78 LEU CB C 39.010 0.04 . 293 138 78 LEU N N 132.080 0.01 . 294 139 79 LYS H H 9.588 0.00 . 295 139 79 LYS C C 175.118 0.00 . 296 139 79 LYS CA C 54.734 0.06 . 297 139 79 LYS CB C 31.201 0.00 . 298 139 79 LYS N N 125.627 0.02 . 299 140 80 ILE H H 9.082 0.00 . 300 140 80 ILE C C 175.668 0.00 . 301 140 80 ILE CA C 61.542 0.08 . 302 140 80 ILE CB C 39.315 0.10 . 303 140 80 ILE N N 125.998 0.03 . 304 141 81 ILE H H 7.771 0.00 . 305 141 81 ILE C C 175.148 0.00 . 306 141 81 ILE CA C 60.245 0.02 . 307 141 81 ILE CB C 38.450 0.21 . 308 141 81 ILE N N 127.094 0.05 . 309 142 82 ASN H H 8.446 0.00 . 310 142 82 ASN C C 174.731 0.00 . 311 142 82 ASN CA C 52.336 0.06 . 312 142 82 ASN CB C 40.033 0.03 . 313 142 82 ASN N N 126.292 0.04 . 314 143 83 TYR H H 8.337 0.00 . 315 143 83 TYR C C 176.839 0.00 . 316 143 83 TYR CA C 60.010 0.07 . 317 143 83 TYR CB C 38.848 0.03 . 318 143 83 TYR N N 124.805 0.05 . 319 144 84 ARG H H 7.486 0.01 . 320 144 84 ARG C C 176.885 0.00 . 321 144 84 ARG CA C 57.319 0.03 . 322 144 84 ARG CB C 30.605 0.01 . 323 144 84 ARG N N 117.142 0.03 . 324 145 85 ASP H H 7.411 0.00 . 325 145 85 ASP C C 176.190 0.00 . 326 145 85 ASP CA C 53.653 0.10 . 327 145 85 ASP CB C 41.967 0.13 . 328 145 85 ASP N N 117.686 0.03 . 329 146 86 ASP H H 9.006 0.01 . 330 146 86 ASP C C 178.998 0.00 . 331 146 86 ASP CA C 57.069 0.05 . 332 146 86 ASP CB C 41.763 0.07 . 333 146 86 ASP N N 126.618 0.05 . 334 147 87 GLU H H 8.546 0.00 . 335 147 87 GLU C C 177.812 0.00 . 336 147 87 GLU CA C 58.351 0.04 . 337 147 87 GLU CB C 29.382 0.06 . 338 147 87 GLU N N 117.990 0.06 . 339 148 88 LYS H H 7.998 0.00 . 340 148 88 LYS C C 177.181 0.00 . 341 148 88 LYS CA C 55.259 0.05 . 342 148 88 LYS CB C 32.413 0.03 . 343 148 88 LYS N N 116.874 0.04 . 344 149 89 SER H H 7.527 0.00 . 345 149 89 SER C C 172.256 0.00 . 346 149 89 SER CA C 60.847 0.10 . 347 149 89 SER CB C 62.843 0.12 . 348 149 89 SER N N 117.618 0.02 . 349 150 90 PHE H H 8.501 0.01 . 350 150 90 PHE C C 173.776 0.00 . 351 150 90 PHE CA C 57.924 0.23 . 352 150 90 PHE CB C 42.777 0.07 . 353 150 90 PHE N N 127.155 0.05 . 354 151 91 SER H H 7.963 0.00 . 355 151 91 SER C C 172.786 0.00 . 356 151 91 SER CA C 56.462 0.10 . 357 151 91 SER CB C 67.367 0.02 . 358 151 91 SER N N 121.273 0.03 . 359 152 92 ARG H H 9.031 0.00 . 360 152 92 ARG C C 174.313 0.00 . 361 152 92 ARG CA C 55.041 0.05 . 362 152 92 ARG CB C 36.988 0.02 . 363 152 92 ARG N N 117.851 0.02 . 364 153 93 ARG H H 8.619 0.00 . 365 153 93 ARG C C 176.607 0.00 . 366 153 93 ARG CA C 55.460 0.07 . 367 153 93 ARG CB C 33.355 0.10 . 368 153 93 ARG N N 120.926 0.02 . 369 154 94 ILE H H 9.118 0.01 . 370 154 94 ILE CA C 59.602 0.04 . 371 154 94 ILE CB C 44.122 0.00 . 372 154 94 ILE N N 112.563 0.04 . 373 155 95 SER C C 175.125 0.00 . 374 156 96 HIS H H 8.618 0.00 . 375 156 96 HIS CA C 56.435 0.00 . 376 156 96 HIS N N 122.867 0.02 . 377 157 97 LEU H H 6.198 0.00 . 378 157 97 LEU N N 118.521 0.00 . 379 158 98 PHE C C 174.791 0.00 . 380 158 98 PHE CA C 53.462 0.04 . 381 158 98 PHE CB C 38.829 0.00 . 382 159 99 PHE H H 7.975 0.00 . 383 159 99 PHE CA C 55.432 0.01 . 384 159 99 PHE CB C 42.534 0.00 . 385 159 99 PHE N N 121.883 0.04 . 386 160 100 HIS H H 8.051 0.00 . 387 160 100 HIS N N 122.417 0.00 . 388 162 102 GLU C C 173.417 0.00 . 389 162 102 GLU CA C 57.972 0.00 . 390 163 103 ASN H H 8.739 0.00 . 391 163 103 ASN CA C 55.461 0.00 . 392 163 103 ASN N N 123.968 0.03 . 393 166 106 GLY C C 176.051 0.00 . 394 167 107 PHE H H 7.745 0.00 . 395 167 107 PHE CA C 54.233 0.14 . 396 167 107 PHE CB C 38.147 0.00 . 397 167 107 PHE N N 118.697 0.05 . 398 169 109 ASN H H 7.319 0.00 . 399 169 109 ASN N N 116.972 0.00 . 400 170 110 PHE H H 8.743 0.00 . 401 170 110 PHE C C 175.775 0.00 . 402 170 110 PHE CA C 59.121 0.00 . 403 170 110 PHE CB C 38.937 0.00 . 404 170 110 PHE N N 119.167 0.00 . 405 171 111 MET H H 7.462 0.00 . 406 171 111 MET C C 173.912 0.00 . 407 171 111 MET CA C 55.080 0.05 . 408 171 111 MET CB C 32.411 0.00 . 409 171 111 MET N N 111.169 0.04 . 410 172 112 ALA H H 9.028 0.01 . 411 172 112 ALA C C 178.471 0.00 . 412 172 112 ALA CA C 53.550 0.07 . 413 172 112 ALA CB C 18.852 0.00 . 414 172 112 ALA N N 126.144 0.07 . 415 173 113 TRP H H 9.085 0.01 . 416 173 113 TRP CA C 60.872 0.07 . 417 173 113 TRP N N 126.899 0.03 . 418 174 114 SER C C 174.937 0.00 . 419 174 114 SER CA C 60.474 0.10 . 420 175 115 GLU H H 6.807 0.00 . 421 175 115 GLU C C 177.033 0.00 . 422 175 115 GLU CA C 58.567 0.02 . 423 175 115 GLU CB C 30.549 0.07 . 424 175 115 GLU N N 120.709 0.02 . 425 176 116 VAL H H 7.233 0.00 . 426 176 116 VAL C C 176.156 0.00 . 427 176 116 VAL CA C 65.127 0.05 . 428 176 116 VAL CB C 31.807 0.00 . 429 176 116 VAL N N 115.922 0.01 . 430 177 117 THR H H 7.296 0.00 . 431 177 117 THR C C 174.142 0.00 . 432 177 117 THR CA C 61.790 0.05 . 433 177 117 THR CB C 69.418 0.04 . 434 177 117 THR N N 102.542 0.03 . 435 178 118 ASP H H 6.926 0.00 . 436 178 118 ASP CA C 52.025 0.02 . 437 178 118 ASP CB C 41.676 0.00 . 438 178 118 ASP N N 123.802 0.03 . 439 179 119 PRO C C 178.453 0.00 . 440 179 119 PRO CA C 65.072 0.03 . 441 179 119 PRO CB C 32.359 0.00 . 442 180 120 GLU H H 8.557 0.00 . 443 180 120 GLU C C 178.518 0.00 . 444 180 120 GLU CA C 57.333 0.03 . 445 180 120 GLU CB C 30.285 0.03 . 446 180 120 GLU N N 116.138 0.04 . 447 181 121 LYS H H 7.789 0.00 . 448 181 121 LYS C C 178.285 0.00 . 449 181 121 LYS CA C 57.349 0.01 . 450 181 121 LYS CB C 33.040 0.00 . 451 181 121 LYS N N 116.536 0.02 . 452 182 122 GLY H H 7.445 0.00 . 453 182 122 GLY C C 172.253 0.00 . 454 182 122 GLY CA C 46.637 0.08 . 455 182 122 GLY N N 104.421 0.02 . 456 183 123 PHE H H 9.056 0.01 . 457 183 123 PHE C C 173.427 0.00 . 458 183 123 PHE CA C 58.643 0.10 . 459 183 123 PHE CB C 39.240 0.03 . 460 183 123 PHE N N 116.950 0.04 . 461 184 124 ILE H H 7.582 0.00 . 462 184 124 ILE C C 173.827 0.00 . 463 184 124 ILE CA C 59.171 0.05 . 464 184 124 ILE CB C 41.991 0.00 . 465 184 124 ILE N N 116.281 0.03 . 466 185 125 ASP H H 8.128 0.00 . 467 185 125 ASP C C 175.708 0.00 . 468 185 125 ASP CA C 53.597 0.03 . 469 185 125 ASP CB C 42.959 0.15 . 470 185 125 ASP N N 126.593 0.01 . 471 186 126 ASP H H 8.964 0.01 . 472 186 126 ASP C C 175.259 0.00 . 473 186 126 ASP CA C 55.574 0.08 . 474 186 126 ASP CB C 39.690 0.03 . 475 186 126 ASP N N 127.912 0.02 . 476 187 127 ASP H H 8.664 0.00 . 477 187 127 ASP C C 173.735 0.00 . 478 187 127 ASP CA C 54.828 0.11 . 479 187 127 ASP CB C 42.366 0.06 . 480 187 127 ASP N N 114.517 0.02 . 481 188 128 LYS H H 7.496 0.00 . 482 188 128 LYS C C 176.341 0.00 . 483 188 128 LYS CA C 54.936 0.05 . 484 188 128 LYS CB C 34.529 0.07 . 485 188 128 LYS N N 115.992 0.04 . 486 189 129 VAL H H 7.898 0.00 . 487 189 129 VAL C C 174.139 0.00 . 488 189 129 VAL CA C 61.245 0.14 . 489 189 129 VAL CB C 35.477 0.02 . 490 189 129 VAL N N 124.331 0.05 . 491 190 130 THR H H 10.217 0.00 . 492 190 130 THR C C 170.725 0.00 . 493 190 130 THR CA C 63.339 0.05 . 494 190 130 THR CB C 70.111 0.12 . 495 190 130 THR N N 125.423 0.03 . 496 191 131 PHE H H 8.785 0.01 . 497 191 131 PHE C C 174.380 0.00 . 498 191 131 PHE CA C 56.332 0.15 . 499 191 131 PHE CB C 41.382 0.02 . 500 191 131 PHE N N 126.824 0.04 . 501 192 132 GLU H H 10.010 0.01 . 502 192 132 GLU C C 173.925 0.00 . 503 192 132 GLU CA C 54.683 0.11 . 504 192 132 GLU CB C 35.580 0.12 . 505 192 132 GLU N N 123.484 0.02 . 506 193 133 VAL H H 8.702 0.00 . 507 193 133 VAL C C 174.089 0.00 . 508 193 133 VAL CA C 59.939 0.03 . 509 193 133 VAL CB C 35.851 0.15 . 510 193 133 VAL N N 124.598 0.02 . 511 194 134 PHE H H 8.320 0.01 . 512 194 134 PHE C C 174.258 0.00 . 513 194 134 PHE CA C 55.180 0.04 . 514 194 134 PHE CB C 41.757 0.29 . 515 194 134 PHE N N 126.669 0.07 . 516 195 135 VAL H H 8.822 0.00 . 517 195 135 VAL C C 171.385 0.00 . 518 195 135 VAL CA C 58.846 0.04 . 519 195 135 VAL CB C 34.617 0.00 . 520 195 135 VAL N N 126.248 0.02 . 521 196 136 GLN H H 8.353 0.00 . 522 196 136 GLN C C 174.360 0.00 . 523 196 136 GLN CA C 54.580 0.04 . 524 196 136 GLN CB C 31.459 0.09 . 525 196 136 GLN N N 124.725 0.07 . 526 197 137 ALA H H 8.496 0.00 . 527 197 137 ALA C C 177.256 0.00 . 528 197 137 ALA CA C 50.643 0.04 . 529 197 137 ALA CB C 22.763 0.00 . 530 197 137 ALA N N 127.945 0.03 . 531 198 138 ASP H H 8.984 0.00 . 532 198 138 ASP C C 174.252 0.00 . 533 198 138 ASP CA C 53.811 0.07 . 534 198 138 ASP CB C 41.995 0.02 . 535 198 138 ASP N N 126.266 0.04 . 536 199 139 ALA H H 8.463 0.00 . 537 199 139 ALA CA C 51.164 0.02 . 538 199 139 ALA CB C 17.530 0.00 . 539 199 139 ALA N N 120.923 0.02 . 540 200 140 PRO C C 174.484 0.00 . 541 201 141 HIS H H 8.998 0.01 . 542 201 141 HIS C C 178.285 0.00 . 543 201 141 HIS CA C 57.337 0.01 . 544 201 141 HIS CB C 32.960 0.00 . 545 201 141 HIS N N 118.238 0.01 . 546 202 142 GLY H H 7.448 0.01 . 547 202 142 GLY C C 174.363 0.00 . 548 202 142 GLY CA C 46.537 0.06 . 549 202 142 GLY N N 104.426 0.01 . 550 203 143 VAL H H 7.576 0.01 . 551 203 143 VAL C C 175.032 0.00 . 552 203 143 VAL CA C 60.782 0.06 . 553 203 143 VAL CB C 33.542 0.00 . 554 203 143 VAL N N 115.357 0.01 . 555 204 144 ALA H H 8.057 0.00 . 556 204 144 ALA C C 175.851 0.00 . 557 204 144 ALA CA C 52.262 0.03 . 558 204 144 ALA CB C 19.378 0.00 . 559 204 144 ALA N N 127.413 0.04 . 560 205 145 TRP H H 7.444 0.00 . 561 205 145 TRP CA C 58.587 0.02 . 562 205 145 TRP CB C 30.120 0.00 . 563 205 145 TRP N N 125.595 0.01 . stop_ save_ save_assigned_chemical_shifts_2 _Saveframe_category assigned_chemical_shifts _Details '15N USP7 TRAF-like domain' loop_ _Experiment_label '2D 1H-15N HSQC' stop_ loop_ _Sample_label $sample_2 stop_ _Sample_conditions_label $sample_conditions_1 _Chem_shift_reference_set_label $chem_shift_reference_2 _Mol_system_component_name 'USP7 TRAF-like domain' _Text_data_format . _Text_data . loop_ _Atom_shift_assign_ID _Residue_author_seq_code _Residue_seq_code _Residue_label _Atom_name _Atom_type _Chem_shift_value _Chem_shift_value_error _Chem_shift_ambiguity_code 1 66 6 ARG H H 7.558 0.00 . 2 66 6 ARG N N 121.508 0.00 . 3 67 7 SER H H 8.840 0.00 . 4 67 7 SER N N 116.547 0.00 . 5 68 8 GLU H H 7.475 0.00 . 6 68 8 GLU N N 116.404 0.00 . 7 69 9 ALA H H 8.348 0.00 . 8 69 9 ALA N N 119.115 0.00 . 9 70 10 THR H H 8.266 0.00 . 10 70 10 THR N N 115.737 0.00 . 11 71 11 PHE H H 9.442 0.00 . 12 71 11 PHE N N 124.803 0.00 . 13 72 12 GLN H H 8.566 0.00 . 14 72 12 GLN N N 116.899 0.00 . 15 73 13 PHE H H 9.507 0.00 . 16 73 13 PHE N N 121.694 0.00 . 17 74 14 THR H H 8.779 0.00 . 18 74 14 THR N N 126.959 0.00 . 19 75 15 VAL H H 9.116 0.00 . 20 75 15 VAL N N 129.594 0.00 . 21 76 16 GLU H H 8.121 0.00 . 22 76 16 GLU N N 125.184 0.00 . 23 77 17 ARG H H 8.901 0.00 . 24 77 17 ARG N N 119.074 0.00 . 25 78 18 PHE H H 9.253 0.00 . 26 78 18 PHE N N 121.871 0.00 . 27 79 19 SER H H 9.522 0.00 . 28 79 19 SER N N 109.990 0.00 . 29 80 20 ARG H H 7.796 0.00 . 30 80 20 ARG N N 120.664 0.00 . 31 81 21 LEU H H 7.939 0.00 . 32 81 21 LEU N N 124.635 0.00 . 33 83 23 GLU H H 7.687 0.00 . 34 83 23 GLU N N 120.133 0.00 . 35 84 24 SER H H 8.102 0.00 . 36 84 24 SER N N 111.751 0.00 . 37 85 25 VAL H H 9.176 0.00 . 38 85 25 VAL N N 120.173 0.00 . 39 86 26 LEU H H 8.092 0.00 . 40 86 26 LEU N N 123.305 0.00 . 41 87 27 SER H H 8.542 0.00 . 42 87 27 SER N N 119.343 0.00 . 43 90 30 CYS H H 8.989 0.00 . 44 90 30 CYS N N 123.294 0.00 . 45 91 31 PHE H H 8.977 0.00 . 46 91 31 PHE N N 128.589 0.00 . 47 92 32 VAL H H 8.557 0.00 . 48 92 32 VAL N N 123.511 0.00 . 49 93 33 ARG H H 9.299 0.00 . 50 93 33 ARG N N 124.390 0.00 . 51 94 34 ASN H H 8.703 0.00 . 52 94 34 ASN N N 109.647 0.00 . 53 95 35 LEU H H 7.744 0.00 . 54 95 35 LEU N N 118.645 0.00 . 55 97 37 TRP H H 8.507 0.00 . 56 97 37 TRP N N 127.197 0.00 . 57 98 38 LYS H H 9.199 0.00 . 58 98 38 LYS N N 117.341 0.00 . 59 99 39 ILE H H 8.529 0.00 . 60 99 39 ILE N N 122.672 0.00 . 61 100 40 MET H H 9.131 0.00 . 62 100 40 MET N N 128.499 0.00 . 63 101 41 VAL H H 8.663 0.00 . 64 101 41 VAL N N 125.966 0.00 . 65 102 42 MET H H 8.624 0.00 . 66 102 42 MET N N 121.007 0.00 . 67 108 48 ASP H H 8.716 0.00 . 68 108 48 ASP N N 113.290 0.00 . 69 109 49 ARG H H 7.512 0.00 . 70 109 49 ARG N N 118.903 0.00 . 71 115 55 VAL H H 8.971 0.00 . 72 115 55 VAL N N 119.906 0.00 . 73 116 56 GLY H H 9.384 0.00 . 74 116 56 GLY N N 117.917 0.00 . 75 117 57 PHE H H 7.155 0.00 . 76 117 57 PHE N N 127.624 0.00 . 77 118 58 PHE H H 9.724 0.00 . 78 118 58 PHE N N 124.157 0.00 . 79 119 59 LEU H H 9.125 0.00 . 80 119 59 LEU N N 123.190 0.00 . 81 120 60 GLN H H 9.833 0.00 . 82 120 60 GLN N N 127.450 0.00 . 83 121 61 CYS H H 9.530 0.00 . 84 121 61 CYS N N 128.538 0.00 . 85 122 62 ASN H H 8.079 0.00 . 86 122 62 ASN N N 122.021 0.00 . 87 123 63 ALA H H 7.470 0.00 . 88 123 63 ALA N N 118.521 0.00 . 89 124 64 GLU H H 8.162 0.00 . 90 124 64 GLU N N 115.187 0.00 . 91 125 65 SER H H 6.796 0.00 . 92 125 65 SER N N 112.553 0.00 . 93 126 66 ASP H H 8.749 0.00 . 94 126 66 ASP N N 126.137 0.00 . 95 127 67 SER H H 8.243 0.00 . 96 127 67 SER N N 114.808 0.00 . 97 129 69 SER H H 8.395 0.00 . 98 129 69 SER N N 115.267 0.00 . 99 130 70 TRP H H 6.948 0.00 . 100 130 70 TRP N N 120.746 0.00 . 101 131 71 SER H H 8.994 0.00 . 102 131 71 SER N N 111.776 0.00 . 103 132 72 CYS H H 9.434 0.00 . 104 132 72 CYS N N 120.960 0.00 . 105 133 73 HIS H H 9.466 0.00 . 106 133 73 HIS N N 133.398 0.00 . 107 134 74 ALA H H 8.507 0.00 . 108 134 74 ALA N N 127.197 0.00 . 109 135 75 GLN H H 8.316 0.00 . 110 135 75 GLN N N 117.220 0.00 . 111 136 76 ALA H H 8.916 0.00 . 112 136 76 ALA N N 122.158 0.00 . 113 137 77 VAL H H 9.094 0.00 . 114 137 77 VAL N N 121.009 0.00 . 115 138 78 LEU H H 9.026 0.00 . 116 138 78 LEU N N 131.749 0.00 . 117 139 79 LYS H H 9.594 0.00 . 118 139 79 LYS N N 125.662 0.00 . 119 140 80 ILE H H 9.093 0.00 . 120 140 80 ILE N N 126.072 0.00 . 121 141 81 ILE H H 7.777 0.00 . 122 141 81 ILE N N 127.178 0.00 . 123 142 82 ASN H H 8.427 0.00 . 124 142 82 ASN N N 126.398 0.00 . 125 143 83 TYR H H 8.342 0.00 . 126 143 83 TYR N N 124.822 0.00 . 127 144 84 ARG H H 7.478 0.00 . 128 144 84 ARG N N 117.335 0.00 . 129 145 85 ASP H H 7.412 0.00 . 130 145 85 ASP N N 117.772 0.00 . 131 146 86 ASP H H 9.011 0.00 . 132 146 86 ASP N N 126.411 0.00 . 133 147 87 GLU H H 8.543 0.00 . 134 147 87 GLU N N 118.046 0.00 . 135 148 88 LYS H H 8.004 0.00 . 136 148 88 LYS N N 116.989 0.00 . 137 149 89 SER H H 7.525 0.00 . 138 149 89 SER N N 117.700 0.00 . 139 150 90 PHE H H 8.507 0.00 . 140 150 90 PHE N N 127.197 0.00 . 141 151 91 SER H H 7.953 0.00 . 142 151 91 SER N N 121.363 0.00 . 143 152 92 ARG H H 9.026 0.00 . 144 152 92 ARG N N 117.566 0.00 . 145 153 93 ARG H H 8.624 0.00 . 146 153 93 ARG N N 121.007 0.00 . 147 154 94 ILE H H 9.141 0.00 . 148 154 94 ILE N N 112.281 0.00 . 149 156 96 HIS H H 8.598 0.00 . 150 156 96 HIS N N 122.846 0.00 . 151 157 97 LEU H H 6.172 0.00 . 152 157 97 LEU N N 117.993 0.00 . 153 159 99 PHE H H 8.002 0.00 . 154 159 99 PHE N N 121.669 0.00 . 155 160 100 HIS H H 8.036 0.00 . 156 160 100 HIS N N 122.297 0.00 . 157 163 103 ASN H H 8.728 0.00 . 158 163 103 ASN N N 123.709 0.00 . 159 167 107 PHE H H 7.722 0.00 . 160 167 107 PHE N N 118.654 0.00 . 161 169 109 ASN H H 7.301 0.00 . 162 169 109 ASN N N 117.188 0.00 . 163 170 110 PHE H H 8.693 0.00 . 164 170 110 PHE N N 119.129 0.00 . 165 171 111 MET H H 7.456 0.00 . 166 171 111 MET N N 111.284 0.00 . 167 172 112 ALA H H 9.011 0.00 . 168 172 112 ALA N N 126.411 0.00 . 169 173 113 TRP H H 9.092 0.00 . 170 173 113 TRP N N 127.049 0.00 . 171 175 115 GLU H H 6.802 0.00 . 172 175 115 GLU N N 120.803 0.00 . 173 176 116 VAL H H 7.232 0.00 . 174 176 116 VAL N N 116.019 0.00 . 175 177 117 THR H H 7.284 0.00 . 176 177 117 THR N N 102.644 0.00 . 177 178 118 ASP H H 6.929 0.00 . 178 178 118 ASP N N 123.921 0.00 . 179 180 120 GLU H H 8.553 0.00 . 180 180 120 GLU N N 116.199 0.00 . 181 181 121 LYS H H 7.784 0.00 . 182 181 121 LYS N N 116.645 0.00 . 183 182 122 GLY H H 7.449 0.00 . 184 182 122 GLY N N 104.452 0.00 . 185 183 123 PHE H H 9.055 0.00 . 186 183 123 PHE N N 116.987 0.00 . 187 184 124 ILE H H 7.579 0.00 . 188 184 124 ILE N N 116.405 0.00 . 189 185 125 ASP H H 8.144 0.00 . 190 185 125 ASP N N 126.693 0.00 . 191 186 126 ASP H H 8.975 0.00 . 192 186 126 ASP N N 128.250 0.00 . 193 187 127 ASP H H 8.661 0.00 . 194 187 127 ASP N N 114.613 0.00 . 195 188 128 LYS H H 7.497 0.00 . 196 188 128 LYS N N 116.066 0.00 . 197 189 129 VAL H H 7.896 0.00 . 198 189 129 VAL N N 124.319 0.00 . 199 190 130 THR H H 10.197 0.00 . 200 190 130 THR N N 125.454 0.00 . 201 191 131 PHE H H 8.779 0.00 . 202 191 131 PHE N N 126.959 0.00 . 203 192 132 GLU H H 10.012 0.00 . 204 192 132 GLU N N 123.532 0.00 . 205 193 133 VAL H H 8.701 0.00 . 206 193 133 VAL N N 124.648 0.00 . 207 194 134 PHE H H 8.289 0.00 . 208 194 134 PHE N N 126.731 0.00 . 209 195 135 VAL H H 8.826 0.00 . 210 195 135 VAL N N 126.254 0.00 . 211 196 136 GLN H H 8.342 0.00 . 212 196 136 GLN N N 124.822 0.00 . 213 197 137 ALA H H 8.506 0.00 . 214 197 137 ALA N N 128.002 0.00 . 215 198 138 ASP H H 9.011 0.00 . 216 198 138 ASP N N 126.411 0.00 . 217 199 139 ALA H H 8.464 0.00 . 218 199 139 ALA N N 120.823 0.00 . 219 201 141 HIS H H 9.017 0.00 . 220 201 141 HIS N N 118.181 0.00 . 221 202 142 GLY H H 7.449 0.00 . 222 202 142 GLY N N 104.452 0.00 . 223 203 143 VAL H H 7.556 0.00 . 224 203 143 VAL N N 115.245 0.00 . 225 204 144 ALA H H 8.052 0.00 . 226 204 144 ALA N N 127.491 0.00 . 227 205 145 TRP H H 7.446 0.00 . 228 205 145 TRP N N 125.714 0.00 . stop_ save_ save_spectral_peak_list_1 _Saveframe_category spectral_peak_list _Details '15N/13C USP7 TRAF-like domain HSQC' _Experiment_label '2D 1H-15N HSQC' _Number_of_spectral_dimensions 2 loop_ _Expt_dimension_ID _Atom_type _Spectral_region 1 H HN 2 N N stop_ _Sample_label $sample_1 _Sample_conditions_label $sample_conditions_1 _Text_data_format "NMR-STAR v3" _Text_data ; >>save_spectral_peak_list_1 >> _Spectral_peak_list.Sf_category spectral_peak_list >> _Spectral_peak_list.Sf_framecode spectral_peak_list_1 >> _Spectral_peak_list.Entry_ID 50080 >> _Spectral_peak_list.ID 1 >> _Spectral_peak_list.Name . >> _Spectral_peak_list.Sample_ID 1 >> _Spectral_peak_list.Sample_label $sample_1 >> _Spectral_peak_list.Sample_condition_list_ID 1 >> _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 >> _Spectral_peak_list.Chem_shift_reference_ID . >> _Spectral_peak_list.Chem_shift_reference_label . >> _Spectral_peak_list.Experiment_ID 5 >> _Spectral_peak_list.Experiment_name '2D 1H-15N HSQC' >> _Spectral_peak_list.Experiment_class . >> _Spectral_peak_list.Experiment_type . >> _Spectral_peak_list.Number_of_spectral_dimensions 2 >> _Spectral_peak_list.Chemical_shift_list . >> _Spectral_peak_list.Assigned_chem_shift_list_ID . >> _Spectral_peak_list.Assigned_chem_shift_list_label . >> _Spectral_peak_list.Details '15N/13C USP7 TRAF-like domain HSQC' >> _Spectral_peak_list.Text_data_format text >> _Spectral_peak_list.Text_data >>; >>Assignment w1 w2 >> >> R66N-H 121.334 7.544 >> S67N-H 116.547 8.840 >> E68N-H 116.313 7.474 >> A69N-H 119.020 8.337 >> T70N-H 115.642 8.270 >> F71N-H 124.675 9.444 >> Q72N-H 116.829 8.567 >> F73N-H 121.642 9.509 >> T74N-H 126.845 8.781 >> V75N-H 129.478 9.114 >> E76N-H 125.118 8.105 >> R77N-H 118.982 8.902 >> F78N-H 121.812 9.254 >> S79N-H 110.002 9.531 >> R80N-H 120.588 7.811 >> L81N-H 124.481 7.932 >> E83N-H 120.075 7.691 >> S84N-H 111.762 8.111 >> V85N-H 120.082 9.179 >> L86N-H 123.285 8.085 >> S87N-H 119.243 8.546 >> C90N-H 123.123 8.965 >> F91N-H 128.521 8.968 >> V92N-H 123.395 8.599 >> R93N-H 124.391 9.306 >> N94N-H 109.438 8.729 >> L95N-H 118.675 7.751 >> W97N-H 126.596 8.517 >> K98N-H 117.291 9.209 >> I99N-H 122.491 8.531 >> M100N-H 128.306 9.087 >> V101N-H 125.956 8.674 >> M102N-H 120.964 8.641 >> D108N-H 113.393 8.702 >> R109N-H 118.812 7.501 >> V115N-H 119.896 8.967 >> G116N-H 117.861 9.379 >> F117N-H 127.685 7.262 >> F118N-H 124.449 9.743 >> L119N-H 122.891 9.136 >> Q120N-H 127.098 9.761 >> C121N-H 128.285 9.444 >> N122N-H 121.930 8.071 >> A123N-H 118.177 7.463 >> E124N-H 115.203 8.170 >> S125N-H 112.493 6.797 >> D126N-H 126.001 8.749 >> S127N-H 114.739 8.265 >> S129N-H 115.636 8.427 >> W130N-H 120.702 6.958 >> S131N-H 111.657 8.950 >> C132N-H 120.994 9.516 >> H133N-H 133.087 9.448 >> A134N-H 127.155 8.595 >> Q135N-H 117.131 8.307 >> A136N-H 122.232 8.929 >> V137N-H 121.019 9.097 >> L138N-H 132.089 9.048 >> K139N-H 125.611 9.588 >> I140N-H 126.033 9.082 >> I141N-H 127.112 7.775 >> N142N-H 126.329 8.444 >> Y143N-H 124.746 8.348 >> R144N-H 117.178 7.480 >> D145N-H 117.706 7.409 >> D146N-H 126.659 9.009 >> E147N-H 118.001 8.545 >> K148N-H 116.894 7.998 >> S149N-H 117.617 7.526 >> F150N-H 127.131 8.495 >> S151N-H 121.267 7.963 >> R152N-H 117.819 9.027 >> R153N-H 120.910 8.622 >> I154N-H 112.570 9.120 >> H156N-H 122.852 8.618 >> L157N-H 118.521 6.198 >> F159N-H 121.899 7.976 >> H160N-H 122.417 8.051 >> N163N-H 123.948 8.739 >> F167N-H 118.710 7.743 >> N169N-H 116.972 7.319 >> F170N-H 119.167 8.743 >> M171N-H 111.214 7.460 >> A172N-H 126.145 9.032 >> W173N-H 126.926 9.081 >> E175N-H 120.726 6.809 >> V176N-H 115.920 7.232 >> T177N-H 102.542 7.295 >> D178N-H 123.821 6.927 >> E180N-H 116.118 8.556 >> K181N-H 116.544 7.789 >> G182N-H 104.400 7.444 >> F183N-H 116.949 9.057 >> I184N-H 116.317 7.582 >> D185N-H 126.603 8.129 >> D186N-H 127.889 8.964 >> D187N-H 114.497 8.665 >> K188N-H 115.992 7.492 >> V189N-H 124.317 7.898 >> T190N-H 125.397 10.218 >> F191N-H 126.841 8.782 >> E192N-H 123.483 10.008 >> V193N-H 124.600 8.703 >> F194N-H 126.672 8.322 >> V195N-H 126.209 8.828 >> Q196N-H 124.746 8.348 >> A197N-H 127.927 8.495 >> D198N-H 126.247 8.982 >> A199N-H 120.886 8.464 >> H201N-H 118.230 9.006 >> G202N-H 104.416 7.465 >> V203N-H 115.356 7.578 >> A204N-H 127.397 8.056 >> W205N-H 125.580 7.443 >>; >> >> loop_ >> _Spectral_dim.ID >> _Spectral_dim.Axis_code >> _Spectral_dim.Spectrometer_frequency >> _Spectral_dim.Atom_type >> _Spectral_dim.Atom_isotope_number >> _Spectral_dim.Spectral_region >> _Spectral_dim.Magnetization_linkage_ID >> _Spectral_dim.Under_sampling_type >> _Spectral_dim.Sweep_width >> _Spectral_dim.Sweep_width_units >> _Spectral_dim.Value_first_point >> _Spectral_dim.Absolute_peak_positions >> _Spectral_dim.Acquisition >> _Spectral_dim.Center_frequency_offset >> _Spectral_dim.Encoding_code >> _Spectral_dim.Encoded_reduced_dimension_ID >> _Spectral_dim.Entry_ID >> _Spectral_dim.Spectral_peak_list_ID >> >> 1 . . H 1 HN . aliased 12019.231 Hz . . . . . . 50080 1 >> 2 . . N 15 N . aliased 2900.022 Hz . . . . . . 50080 1 >> >> stop_ >> >>save_ >> ; save_ save_spectral_peak_list_2 _Saveframe_category spectral_peak_list _Details '15N/13C USP7 TRAF-like domain HNCACB' _Experiment_label '3D HNCACB' _Number_of_spectral_dimensions 3 loop_ _Expt_dimension_ID _Atom_type _Spectral_region 1 H HN 2 C C 3 N N stop_ _Sample_label $sample_1 _Sample_conditions_label $sample_conditions_1 _Text_data_format "NMR-STAR v3" _Text_data ; >>save_spectral_peak_list_2 >> _Spectral_peak_list.Sf_category spectral_peak_list >> _Spectral_peak_list.Sf_framecode spectral_peak_list_2 >> _Spectral_peak_list.Entry_ID 50080 >> _Spectral_peak_list.ID 2 >> _Spectral_peak_list.Name . >> _Spectral_peak_list.Sample_ID 1 >> _Spectral_peak_list.Sample_label $sample_1 >> _Spectral_peak_list.Sample_condition_list_ID 1 >> _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 >> _Spectral_peak_list.Chem_shift_reference_ID . >> _Spectral_peak_list.Chem_shift_reference_label . >> _Spectral_peak_list.Experiment_ID 3 >> _Spectral_peak_list.Experiment_name '3D HNCACB' >> _Spectral_peak_list.Experiment_class . >> _Spectral_peak_list.Experiment_type . >> _Spectral_peak_list.Number_of_spectral_dimensions 3 >> _Spectral_peak_list.Chemical_shift_list . >> _Spectral_peak_list.Assigned_chem_shift_list_ID . >> _Spectral_peak_list.Assigned_chem_shift_list_label . >> _Spectral_peak_list.Details '15N/13C USP7 TRAF-like domain HNCACB' >> _Spectral_peak_list.Text_data_format text >> _Spectral_peak_list.Text_data >>; >>Assignment w1 w2 w3 >> >> R66N-CA-H 121.282 56.179 7.548 >> R66N-CB-H 121.334 31.107 7.539 >> S67N-R66CA-S67H 116.404 56.191 8.830 >> S67N-CB-H 116.547 64.479 8.820 >> E68N-S67CA-E68H 116.290 59.549 7.481 >> E68N-S67CB-E68H 116.313 64.513 7.474 >> E68N-CA-H 116.238 53.793 7.471 >> E68N-CB-H 116.290 33.742 7.470 >> A69N-E68CA-A69H 119.015 53.621 8.335 >> A69N-E68CB-A69H 119.033 33.741 8.329 >> A69N-CA-H 119.028 52.788 8.335 >> A69N-CB-H 119.052 23.759 8.333 >> T70N-A69CA-T70H 115.602 52.745 8.266 >> T70N-A69CB-T70H 115.630 23.862 8.263 >> T70N-CA-H 115.655 61.606 8.264 >> T70N-CB-H 115.631 70.083 8.262 >> F71N-T70CA-F71H 124.784 61.628 9.443 >> F71N-T70CB-F71H 124.667 70.111 9.443 >> F71N-CA-H 124.621 55.954 9.438 >> F71N-CB-H 124.662 41.306 9.438 >> Q72N-F71CA-Q72H 116.809 55.964 8.567 >> Q72N-F71CB-Q72H 116.802 41.325 8.570 >> Q72N-CA-H 116.815 53.860 8.564 >> Q72N-CB-H 116.803 33.249 8.564 >> F73N-Q72CA-F73H 121.580 53.993 9.508 >> F73N-Q72CB-F73H 121.733 33.189 9.517 >> F73N-CA-H 121.578 55.536 9.507 >> F73N-CB-H 121.588 43.921 9.515 >> T74N-F73CB-T74H 126.871 43.931 8.775 >> T74N-CA-H 126.860 62.176 8.775 >> T74N-CB-H 126.860 69.991 8.775 >> V75N-T74CA-V75H 129.395 62.183 9.115 >> V75N-T74CB-V75H 129.478 69.928 9.111 >> V75N-CA-H 129.584 62.246 9.109 >> V75N-CB-H 129.428 33.014 9.098 >> E76N-V75CA-E76H 125.159 62.087 8.096 >> E76N-V75CB-E76H 125.168 33.231 8.106 >> E76N-CA-H 125.138 55.527 8.107 >> E76N-CB-H 125.147 31.065 8.107 >> R77N-E76CA-R77H 118.977 55.658 8.898 >> R77N-E76CB-R77H 118.950 31.298 8.904 >> R77N-CA-H 118.976 56.500 8.893 >> R77N-CB-H 118.972 27.913 8.905 >> F78N-R77CA-F78H 121.846 56.464 9.250 >> F78N-R77CB-F78H 121.785 27.955 9.253 >> F78N-CA-H 121.816 63.418 9.251 >> F78N-CB-H 121.810 40.058 9.246 >> R80N-CA-H 120.555 54.796 7.810 >> R80N-CB-H 120.588 30.309 7.808 >> L81N-R80CA-L81H 124.540 54.822 7.922 >> L81N-CA-H 124.408 57.534 7.937 >> L81N-CB-H 124.574 43.024 7.925 >> E83N-S82CA-E83H 120.218 57.989 7.707 >> E83N-S82CB-E83H 120.070 65.017 7.696 >> E83N-CA-H 120.105 54.605 7.687 >> E83N-CB-H 120.109 32.335 7.690 >> S84N-E83CA-S84H 111.663 54.713 8.109 >> S84N-E83CB-S84H 111.724 32.265 8.113 >> S84N-CA-H 111.775 58.098 8.107 >> S84N-CB-H 111.766 64.517 8.105 >> V85N-S84CB-V85H 120.290 64.737 9.176 >> V85N-CA-H 120.128 60.230 9.154 >> V85N-CB-H 120.275 35.733 9.188 >> L86N-V85CA-L86H 123.181 60.198 8.093 >> L86N-V85CB-L86H 123.319 35.539 8.087 >> L86N-CA-H 123.245 52.955 8.088 >> L86N-CB-H 123.217 46.481 8.084 >> S87N-L86CA-S87H 119.302 52.959 8.544 >> S87N-L86CB-S87H 119.317 46.512 8.549 >> S87N-CA-H 119.295 57.283 8.553 >> S87N-CB-H 119.200 63.370 8.547 >> C90N-P89CA-C90H 123.161 62.320 8.966 >> C90N-P89CB-C90H 123.093 32.658 8.946 >> C90N-CA-H 123.161 57.058 8.960 >> C90N-CB-H 123.118 27.208 8.970 >> F91N-C90CA-F91H 128.495 57.064 8.969 >> F91N-C90CB-F91H 128.540 27.264 8.956 >> F91N-CA-H 128.513 58.548 8.968 >> F91N-CB-H 128.495 40.095 8.965 >> V92N-F91CA-V92H 123.480 58.554 8.607 >> V92N-F91CB-V92H 123.422 40.193 8.597 >> V92N-CA-H 123.438 62.999 8.595 >> V92N-CB-H 123.395 34.826 8.601 >> R93N-V92CA-R93H 124.319 63.048 9.305 >> R93N-CA-H 124.358 56.806 9.303 >> R93N-CB-H 124.360 27.226 9.298 >> N94N-R93CA-N94H 109.438 56.914 8.723 >> N94N-R93CB-N94H 109.279 27.463 8.735 >> N94N-CA-H 109.438 54.431 8.727 >> N94N-CB-H 109.473 38.199 8.719 >> L95N-N94CA-L95H 118.745 54.370 7.749 >> L95N-N94CB-L95H 118.604 38.147 7.749 >> L95N-CA-H 118.688 51.310 7.749 >> L95N-CB-H 118.721 44.169 7.747 >> W97N-P96CA-W97H 126.450 61.544 8.518 >> W97N-P96CB-W97H 126.596 31.570 8.516 >> W97N-CA-H 126.567 55.270 8.523 >> W97N-CB-H 126.573 29.788 8.505 >> K98N-W97CB-K98H 117.300 29.697 9.215 >> K98N-CA-H 117.314 55.032 9.210 >> K98N-CB-H 117.172 38.742 9.210 >> I99N-K98CA-I99H 122.391 54.945 8.536 >> I99N-CA-H 122.361 62.041 8.541 >> I99N-CB-H 122.472 41.377 8.532 >> M100N-CA-H 128.440 54.359 9.103 >> M100N-CB-H 128.222 37.315 9.096 >> V101N-CB-H 125.827 35.758 8.663 >> M102N-CA-H 120.873 53.430 8.630 >>D108N-P107CA-D108H 113.458 64.918 8.696 >> D108N-CA-H 113.355 54.294 8.697 >> D108N-CB-H 113.489 40.221 8.687 >> R109N-CA-H 118.742 56.636 7.503 >> R109N-CB-H 118.736 29.426 7.503 >>V115N-S114CA-V115H 119.895 57.766 8.973 >>V115N-S114CB-V115H 119.896 67.860 8.983 >> V115N-CA-H 119.863 61.997 8.973 >> V115N-CB-H 119.896 33.897 8.978 >>G116N-V115CA-G116H 117.861 62.009 9.378 >> G116N-CA-H 117.861 45.258 9.380 >> F118N-CB-H 124.449 43.413 9.741 >>L119N-F118CA-L119H 122.938 55.898 9.121 >> L119N-CA-H 122.914 53.414 9.139 >>Q120N-L119CA-Q120H 127.098 53.269 9.763 >> Q120N-CA-H 127.153 54.177 9.765 >>C121N-Q120CA-C121H 128.111 54.125 9.424 >> C121N-CA-H 128.328 56.383 9.439 >>N122N-C121CA-N122H 121.930 56.579 8.069 >> N122N-CA-H 122.038 53.288 8.075 >> N122N-CB-H 121.978 39.071 8.081 >>A123N-N122CA-A123H 118.201 53.375 7.455 >> A123N-CA-H 118.186 54.486 7.465 >> A123N-CB-H 118.212 19.525 7.469 >>E124N-A123CA-E124H 115.143 54.810 8.168 >>E124N-A123CB-E124H 115.203 19.730 8.168 >> E124N-CA-H 115.150 56.347 8.173 >> E124N-CB-H 115.151 29.545 8.168 >>S125N-E124CA-S125H 112.555 56.863 6.801 >>S125N-E124CB-S125H 112.525 29.286 6.804 >> S125N-CA-H 112.446 57.678 6.799 >> S125N-CB-H 112.501 63.651 6.800 >> D126N-CA-H 125.974 53.811 8.739 >> D126N-CB-H 126.031 40.596 8.764 >>S127N-D126CA-S127H 114.795 53.942 8.268 >>S127N-D126CB-S127H 114.796 40.614 8.260 >> S127N-CA-H 114.778 57.664 8.267 >> S127N-CB-H 114.779 63.442 8.262 >> S129N-CB-H 115.636 64.721 8.421 >>W130N-S129CA-W130H 120.701 58.546 6.955 >>W130N-S129CB-W130H 120.759 64.827 6.967 >> W130N-CA-H 120.662 55.092 6.956 >> W130N-CB-H 120.688 30.622 6.957 >>S131N-W130CA-S131H 111.657 55.060 8.959 >>S131N-W130CB-S131H 111.637 30.557 8.936 >> S131N-CA-H 111.690 58.949 8.951 >> S131N-CB-H 111.679 65.291 8.944 >>C132N-S131CA-C132H 120.991 59.021 9.517 >>C132N-S131CB-C132H 120.994 65.594 9.516 >> C132N-CA-H 120.941 60.291 9.514 >> C132N-CB-H 120.992 30.272 9.524 >>H133N-C132CA-H133H 133.087 60.301 9.444 >> H133N-CA-H 133.087 57.524 9.439 >> H133N-CB-H 133.056 30.988 9.448 >>A134N-H133CA-A134H 127.038 57.498 8.594 >> A134N-CA-H 127.262 51.398 8.594 >> A134N-CB-H 127.154 24.393 8.599 >>Q135N-A134CA-Q135H 117.117 51.453 8.319 >>Q135N-A134CB-Q135H 117.131 24.438 8.310 >> Q135N-CA-H 117.117 54.019 8.302 >> Q135N-CB-H 117.079 32.027 8.306 >>A136N-Q135CA-A136H 122.334 53.915 8.935 >>A136N-Q135CB-A136H 122.232 32.062 8.937 >> A136N-CA-H 122.304 50.584 8.936 >> A136N-CB-H 122.300 23.892 8.921 >>V137N-A136CA-V137H 121.019 50.683 9.099 >>V137N-A136CB-V137H 120.951 23.818 9.113 >> V137N-CA-H 120.987 62.440 9.098 >> V137N-CB-H 121.019 33.972 9.103 >>L138N-V137CB-L138H 132.089 33.983 9.047 >> L138N-CB-H 132.089 38.973 9.045 >>K139N-L138CA-K139H 125.611 55.398 9.592 >>K139N-L138CB-K139H 125.664 39.046 9.579 >> K139N-CA-H 125.628 54.651 9.585 >> K139N-CB-H 125.611 31.201 9.592 >>I140N-K139CA-M100H 125.944 54.809 9.094 >> I140N-CA-H 125.996 61.615 9.078 >> I140N-CB-H 125.978 39.414 9.079 >>I141N-I140CA-I141H 126.974 61.398 7.773 >>I141N-I140CB-I141H 127.174 39.216 7.772 >> I141N-CA-H 127.066 60.225 7.763 >> I141N-CB-H 127.109 38.236 7.771 >>N142N-I141CA-N142H 126.360 60.234 8.452 >>N142N-I141CB-N142H 126.227 38.663 8.445 >> N142N-CA-H 126.261 52.282 8.439 >> N142N-CB-H 126.253 40.066 8.450 >>Y143N-N142CA-Y143H 124.845 52.285 8.334 >>Y143N-N142CB-Y143H 124.866 40.000 8.337 >> Y143N-CA-H 124.815 59.913 8.330 >> Y143N-CB-H 124.867 38.821 8.337 >>R144N-Y143CA-R144H 117.080 60.027 7.497 >>R144N-Y143CB-R144H 117.179 38.875 7.483 >> R144N-CA-H 117.114 57.305 7.484 >> R144N-CB-H 117.140 30.612 7.491 >>D145N-R144CA-D145H 117.679 57.271 7.410 >>D145N-R144CB-D145H 117.643 30.598 7.412 >> D145N-CA-H 117.696 53.523 7.410 >> D145N-CB-H 117.644 42.102 7.410 >>D146N-D145CA-D146H 126.659 53.779 9.001 >>D146N-D145CB-D146H 126.571 41.832 9.014 >> D146N-CA-H 126.541 57.019 8.995 >> D146N-CB-H 126.571 41.832 9.014 >>E147N-D146CA-E147H 118.025 57.025 8.546 >>E147N-D146CB-E147H 117.947 41.693 8.547 >> E147N-CA-H 117.969 58.340 8.548 >> E147N-CB-H 117.940 29.326 8.542 >>K148N-E147CA-K148H 116.803 58.302 7.994 >>K148N-E147CB-K148H 116.810 29.438 7.997 >> K148N-CA-H 116.948 55.182 7.997 >> K148N-CB-H 116.879 32.381 7.999 >>S149N-K148CA-S149H 117.672 55.300 7.533 >>S149N-K148CB-S149H 117.617 32.444 7.522 >> S149N-CA-H 117.626 60.908 7.527 >> S149N-CB-H 117.607 62.959 7.525 >>F150N-S149CA-F150H 127.212 60.672 8.510 >>F150N-S149CB-F150H 127.131 62.726 8.515 >> F150N-CB-H 127.099 42.703 8.496 >>S151N-F150CA-S151H 121.260 57.621 7.960 >>S151N-F150CB-S151H 121.340 42.851 7.970 >> S151N-CA-H 121.252 56.600 7.960 >> S151N-CB-H 121.285 67.345 7.963 >>R152N-S151CA-R152H 117.894 56.308 9.026 >>R152N-S151CB-R152H 117.868 67.388 9.039 >> R152N-CA-H 117.832 55.088 9.038 >> R152N-CB-H 117.866 37.011 9.029 >>R153N-R152CB-R153H 120.932 36.965 8.618 >> R153N-CB-H 120.911 33.457 8.625 >>I154N-R153CA-I154H 112.569 55.559 9.119 >>I154N-R153CB-I154H 112.574 33.252 9.105 >> I154N-CA-H 112.462 59.644 9.121 >> I154N-CB-H 112.574 44.122 9.111 >>F159N-F158CA-F159H 121.807 53.417 7.973 >>F159N-F158CB-F159H 121.915 38.829 7.977 >> F159N-CA-H 121.838 55.440 7.971 >> F159N-CB-H 121.899 42.534 7.972 >> F167N-CA-H 118.694 54.096 7.746 >> F167N-CB-H 118.604 38.147 7.749 >>M171N-F170CB-M171H 111.187 38.937 7.469 >> M171N-CA-H 111.093 55.049 7.460 >> M171N-CB-H 111.141 32.411 7.453 >> A172N-CA-H 126.270 53.439 9.015 >> A172N-CB-H 126.168 18.852 9.029 >>W173N-A172CA-W173H 126.882 53.577 9.084 >> W173N-CA-H 126.926 60.941 9.072 >>E175N-S174CA-E175H 120.742 60.378 6.795 >> E175N-CA-H 120.686 58.574 6.809 >> E175N-CB-H 120.705 30.614 6.806 >>V176N-E175CA-V176H 115.914 58.546 7.229 >>V176N-E175CB-V176H 115.922 30.484 7.238 >> V176N-CA-H 115.905 65.087 7.234 >> V176N-CB-H 115.946 31.807 7.234 >>T177N-V176CA-T177H 102.605 65.204 7.293 >> T177N-CA-H 102.490 61.876 7.295 >> T177N-CB-H 102.554 69.381 7.300 >>D178N-T177CA-D178H 123.821 61.788 6.924 >>D178N-T177CB-D178H 123.821 69.455 6.924 >> D178N-CA-H 123.834 52.005 6.928 >> D178N-CB-H 123.765 41.676 6.926 >>E180N-P179CA-E180H 116.194 65.037 8.561 >>E180N-P179CB-E180H 116.067 32.359 8.554 >> E180N-CA-H 116.170 57.335 8.557 >> E180N-CB-H 116.146 30.258 8.557 >>K181N-E180CA-K181H 116.531 57.290 7.789 >>K181N-E180CB-K181H 116.573 30.313 7.787 >> K181N-CA-H 116.535 57.340 7.788 >> K181N-CB-H 116.502 33.040 7.797 >>G182N-K181CA-G182H 104.402 57.369 7.451 >> G182N-CA-H 104.435 46.624 7.442 >>F183N-G182CA-F183H 116.881 46.609 9.048 >> F183N-CA-H 117.002 58.743 9.059 >> F183N-CB-H 116.921 39.206 9.046 >>I184N-F183CA-I184H 116.317 58.471 7.578 >>I184N-F183CB-I184H 116.228 39.275 7.586 >> I184N-CA-H 116.262 59.090 7.584 >> I184N-CB-H 116.259 41.991 7.585 >>D185N-I184CA-D185H 126.616 59.230 8.136 >> D185N-CA-H 126.584 53.601 8.127 >> D185N-CB-H 126.570 42.810 8.123 >>D185N-F194CB-D185H 126.603 42.156 8.125 >>D186N-D185CB-D186H 127.945 43.107 8.959 >> D186N-CB-H 127.889 39.661 8.977 >>D187N-D186CA-D187H 114.542 55.461 8.660 >>D187N-D186CB-D187H 114.522 39.719 8.665 >> D187N-CA-H 114.522 54.707 8.669 >> D187N-CB-H 114.494 42.307 8.662 >>K188N-D187CA-K188H 115.970 54.911 7.494 >>K188N-D187CB-K188H 116.089 42.425 7.498 >> K188N-CA-H 115.972 54.942 7.496 >> K188N-CB-H 115.958 34.597 7.498 >>V189N-K188CA-V189H 124.295 54.849 7.896 >>V189N-K188CB-V189H 124.448 34.460 7.898 >> V189N-CA-H 124.311 61.114 7.900 >> V189N-CB-H 124.330 35.493 7.892 >>T190N-V189CA-T190H 125.398 61.473 10.216 >>T190N-V189CB-T190H 125.397 35.460 10.217 >> T190N-CA-H 125.446 63.323 10.223 >> T190N-CB-H 125.476 70.231 10.219 >>F191N-T190CA-F191H 126.845 63.279 8.784 >>F191N-T190CB-F191H 126.860 69.991 8.775 >> F191N-CA-H 126.761 56.446 8.795 >> F191N-CB-H 126.845 41.359 8.783 >>E192N-F191CA-E192H 123.493 56.070 10.014 >>E192N-F191CB-E192H 123.469 41.405 10.015 >> E192N-CA-H 123.468 54.766 10.004 >> E192N-CB-H 123.521 35.455 10.020 >>V193N-E192CA-V193H 124.647 54.491 8.706 >>V193N-E192CB-V193H 124.577 35.705 8.703 >> V193N-CA-H 124.601 59.940 8.698 >> V193N-CB-H 124.577 35.705 8.703 >>F194N-V193CA-F194H 126.563 59.899 8.310 >>F194N-V193CB-F194H 126.672 35.997 8.322 >> F194N-CA-H 126.753 55.146 8.316 >> F194N-CB-H 126.785 41.505 8.329 >>V195N-F194CA-V195H 126.285 55.141 8.826 >>V195N-F194CB-V195H 126.268 41.611 8.815 >> V195N-CA-H 126.262 58.813 8.824 >> V195N-CB-H 126.256 34.617 8.815 >>Q196N-V195CA-Q196H 124.668 58.815 8.357 >> Q196N-CA-H 124.804 54.559 8.358 >> Q196N-CB-H 124.838 31.369 8.356 >> Q196N-V195?-H 124.627 34.489 8.347 >>A197N-Q196CA-A197H 128.028 54.533 8.493 >>A197N-Q196CB-A197H 127.927 31.549 8.497 >> A197N-CA-H 127.941 50.577 8.492 >> A197N-CB-H 127.919 22.765 8.497 >>D198N-A197CA-D198H 126.204 50.677 8.982 >>D198N-A197CB-D198H 126.257 22.760 8.989 >> D198N-CA-H 126.276 53.900 8.984 >> D198N-CB-H 126.369 42.011 8.988 >>A199N-D198CA-A199H 120.958 53.718 8.469 >>A199N-D198CB-A199H 120.939 41.978 8.460 >> A199N-CA-H 120.906 51.139 8.460 >> A199N-CB-H 120.917 17.530 8.462 >> H201N-CA-H 118.246 57.326 8.990 >>G202N-H201CA-G202H 104.444 57.349 7.446 >>G202N-H201CB-G202H 104.411 32.960 7.441 >> G202N-CA-H 104.425 46.579 7.448 >>V203N-G202CA-V203H 115.348 46.549 7.576 >> V203N-CA-H 115.373 60.818 7.576 >> V203N-CB-H 115.340 33.542 7.582 >>A204N-V203CA-A204H 127.407 60.682 8.057 >> A204N-CA-H 127.488 52.229 8.061 >> A204N-CB-H 127.427 19.379 8.065 >>W205N-A204CA-W205H 125.589 52.230 7.444 >>W205N-A204CB-W205H 125.616 19.376 7.444 >> W205N-CA-H 125.597 58.571 7.444 >> W205N-CB-H 125.598 30.120 7.444 >>; >> >> loop_ >> _Spectral_dim.ID >> _Spectral_dim.Axis_code >> _Spectral_dim.Spectrometer_frequency >> _Spectral_dim.Atom_type >> _Spectral_dim.Atom_isotope_number >> _Spectral_dim.Spectral_region >> _Spectral_dim.Magnetization_linkage_ID >> _Spectral_dim.Under_sampling_type >> _Spectral_dim.Sweep_width >> _Spectral_dim.Sweep_width_units >> _Spectral_dim.Value_first_point >> _Spectral_dim.Absolute_peak_positions >> _Spectral_dim.Acquisition >> _Spectral_dim.Center_frequency_offset >> _Spectral_dim.Encoding_code >> _Spectral_dim.Encoded_reduced_dimension_ID >> _Spectral_dim.Entry_ID >> _Spectral_dim.Spectral_peak_list_ID >> >> 1 . . H 15 HN . aliased 12019.231 Hz . . . . . . 50080 2 >> 2 . . C 13 C . aliased 12000.000 Hz . . . . . . 50080 2 >> 3 . . N 1 N . aliased 2900.022 Hz . . . . . . 50080 2 >> >> stop_ >> >>save_ >> ; save_ save_spectral_peak_list_3 _Saveframe_category spectral_peak_list _Details '15N/13C USP7 TRAF-like domain HNCA' _Experiment_label '3D HNCA' _Number_of_spectral_dimensions 3 loop_ _Expt_dimension_ID _Atom_type _Spectral_region 1 H HN 2 C C 3 N N stop_ _Sample_label $sample_1 _Sample_conditions_label $sample_conditions_1 _Text_data_format "NMR-STAR v3" _Text_data ; >>save_spectral_peak_list_3 >> _Spectral_peak_list.Sf_category spectral_peak_list >> _Spectral_peak_list.Sf_framecode spectral_peak_list_3 >> _Spectral_peak_list.Entry_ID 50080 >> _Spectral_peak_list.ID 3 >> _Spectral_peak_list.Name . >> _Spectral_peak_list.Sample_ID 1 >> _Spectral_peak_list.Sample_label $sample_1 >> _Spectral_peak_list.Sample_condition_list_ID 1 >> _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 >> _Spectral_peak_list.Chem_shift_reference_ID . >> _Spectral_peak_list.Chem_shift_reference_label . >> _Spectral_peak_list.Experiment_ID 2 >> _Spectral_peak_list.Experiment_name '3D HNCA' >> _Spectral_peak_list.Experiment_class . >> _Spectral_peak_list.Experiment_type . >> _Spectral_peak_list.Number_of_spectral_dimensions 3 >> _Spectral_peak_list.Chemical_shift_list . >> _Spectral_peak_list.Assigned_chem_shift_list_ID . >> _Spectral_peak_list.Assigned_chem_shift_list_label . >> _Spectral_peak_list.Details '15N/13C USP7 TRAF-like domain HNCA' >> _Spectral_peak_list.Text_data_format text >> _Spectral_peak_list.Text_data >>; >>Assignment w1 w2 w3 >> >> R66N-W65CA-R66H 121.334 56.680 7.547 >> R66N-CA-H 121.308 56.109 7.546 >> S67N-R66CA-S67H 116.424 56.119 8.833 >> S67N-CA-H 116.547 59.512 8.845 >> E68N-S67CA-E68H 116.290 59.560 7.473 >> E68N-CA-H 116.290 53.875 7.472 >> A69N-E68CA-A69H 119.015 53.799 8.330 >> A69N-CA-H 119.028 52.897 8.335 >> T70N-A69CA-T70H 115.665 52.896 8.267 >> T70N-CA-H 115.649 61.654 8.266 >> F71N-T70CA-F71H 124.643 61.643 9.438 >> F71N-CA-H 124.642 55.989 9.443 >> Q72N-F71CA-Q72H 116.795 55.964 8.566 >> Q72N-CA-H 116.829 53.889 8.572 >> F73N-Q72CA-F73H 121.713 53.815 9.515 >> F73N-CA-H 121.624 55.735 9.510 >> T74N-F73CA-T74H 126.843 55.729 8.774 >> T74N-CA-H 126.845 62.309 8.779 >> V75N-T74CA-V75H 129.499 62.193 9.111 >> V75N-CA-H 129.440 62.166 9.109 >> E76N-V75CA-E76H 125.116 62.128 8.106 >> E76N-CA-H 125.118 55.513 8.105 >> R77N-E76CA-R77H 118.991 55.512 8.900 >> R77N-CA-H 118.970 56.466 8.899 >> F78N-R77CA-F78H 121.810 56.471 9.249 >> F78N-CA-H 121.807 63.435 9.250 >> S79N-F78CA-S79H 110.043 63.428 9.532 >> S79N-CA-H 109.991 61.897 9.536 >> R80N-S79CA-R80H 120.648 61.853 7.821 >> R80N-CA-H 120.656 54.831 7.809 >> L81N-R80CA-L81H 124.499 54.752 7.932 >> L81N-CA-H 124.558 57.531 7.927 >> E83N-S82CA-E83H 120.024 58.084 7.695 >> E83N-CA-H 120.091 54.684 7.690 >> S84N-E83CA-S84H 111.730 54.686 8.110 >> S84N-CA-H 111.747 58.144 8.108 >> V85N-S84CA-V85H 120.082 58.333 9.188 >> V85N-CA-H 120.116 60.424 9.170 >> L86N-V85CA-L86H 123.257 60.377 8.085 >> L86N-CA-H 123.259 53.041 8.086 >> S87N-L86CA-S87H 119.261 53.035 8.549 >> S87N-CA-H 119.264 57.406 8.551 >> C90N-P89CA-C90H 123.161 62.320 8.966 >> C90N-CA-H 123.161 57.058 8.960 >> F91N-C90CA-F91H 128.495 57.064 8.969 >> F91N-CA-H 128.513 58.548 8.968 >> V92N-F91CA-V92H 123.395 58.553 8.604 >> V92N-CA-H 123.395 63.073 8.602 >> R93N-V92CA-R93H 124.319 63.048 9.305 >> R93N-CA-H 124.358 56.806 9.303 >> N94N-R93CA-N94H 109.438 56.914 8.723 >> N94N-CA-H 109.438 54.431 8.727 >> L95N-N94CA-L95H 118.745 54.370 7.749 >> L95N-CA-H 118.677 51.343 7.750 >> W97N-CA-H 126.564 55.198 8.512 >> W97N-P98?-H 126.563 61.514 8.517 >> K98N-CA-H 117.312 55.081 9.207 >> K98N-W97?-H 117.312 55.081 9.207 >> I99N-K98CA-I99H 122.436 55.015 8.542 >> I99N-CA-H 122.418 61.943 8.534 >>M100N-I99CA-M100H 128.278 61.859 9.087 >> M100N-CA-H 128.261 54.352 9.087 >>V101N-M100CA-V101H 125.977 54.359 8.672 >> V101N-CA-H 125.937 60.162 8.666 >>M102N-V101CA-M102H 120.871 60.181 8.637 >> M102N-CA-H 120.933 53.516 8.632 >>D108N-P107CA-D108H 113.458 64.918 8.696 >> D108N-CA-H 113.355 54.294 8.697 >>R109N-P108CA-R109H 119.007 60.918 7.525 >> R109N-CA-H 118.782 56.697 7.505 >>V115N-S114CA-V115H 119.840 57.595 8.966 >> V115N-CA-H 119.850 62.090 8.967 >>G116N-V115CA-G116H 117.889 61.950 9.381 >> G116N-CA-H 117.702 45.451 9.378 >> F117N-CA-H 127.684 55.478 7.250 >>F118N-F117CA-F118H 124.370 55.990 9.745 >> F118N-CA-H 124.370 55.990 9.745 >>L119N-F118CA-L119H 122.924 55.844 9.135 >> L119N-CA-H 122.904 53.453 9.148 >>Q120N-L119CA-Q120H 127.098 53.269 9.763 >> Q120N-CA-H 127.153 54.177 9.765 >>C121N-Q120CA-C121H 128.111 54.125 9.424 >> C121N-CA-H 128.328 56.383 9.439 >>N122N-C121CA-N122H 121.930 56.579 8.069 >> N122N-CA-H 122.038 53.288 8.075 >>A123N-N122CA-A123H 118.202 53.288 7.463 >> A123N-CA-H 118.184 54.646 7.458 >>E124N-A123CA-E124H 115.199 54.698 8.171 >> E124N-CA-H 115.169 56.543 8.170 >>S125N-E124CA-S125H 112.478 56.488 6.798 >> S125N-CA-H 112.478 57.685 6.799 >> D126N-CA-H 125.988 53.881 8.749 >>S127N-D126CA-S127H 114.740 54.096 8.259 >> S127N-CA-H 114.750 57.677 8.262 >> S129N-CA-H 115.653 58.739 8.423 >>W130N-S129CA-W130H 120.667 58.589 6.957 >> W130N-CA-H 120.673 55.140 6.957 >>S131N-W130CA-S131H 111.657 55.147 8.946 >> S131N-CA-H 111.657 59.015 8.946 >>C132N-S131CA-C132H 120.954 58.877 9.516 >> C132N-CA-H 120.979 60.344 9.516 >>H133N-C132CA-H133H 133.020 60.301 9.456 >> H133N-CA-H 133.054 57.508 9.446 >>A134N-H133CA-A134H 127.130 57.528 8.600 >> A134N-CA-H 127.155 51.618 8.601 >>Q135N-A134CA-Q135H 117.068 51.460 8.312 >> Q135N-CA-H 117.093 54.075 8.307 >>A136N-Q135CA-A136H 122.318 54.175 8.923 >> A136N-CA-H 122.231 50.749 8.927 >>V137N-A136CA-V137H 120.978 50.788 9.101 >> V137N-CA-H 120.998 62.481 9.098 >>L138N-V137CA-L138H 132.056 62.406 9.047 >> L138N-CA-H 132.082 55.279 9.055 >>K139N-L138CA-K139H 125.640 55.234 9.587 >> K139N-CA-H 125.619 54.696 9.587 >>I140N-K139CA-I140H 126.033 54.780 9.085 >> I140N-CA-H 126.000 61.588 9.086 >>I141N-I140CA-I141H 127.105 61.568 7.771 >> I141N-CA-H 127.109 60.262 7.772 >>N142N-I141CA-N142H 126.315 60.258 8.444 >> N142N-CA-H 126.302 52.411 8.450 >>Y143N-N142CA-Y143H 124.813 52.367 8.337 >> Y143N-CA-H 124.746 60.001 8.333 >>R144N-Y143CA-R144H 117.113 60.100 7.490 >> R144N-CA-H 117.156 57.363 7.485 >>D145N-R144CA-D145H 117.706 57.336 7.410 >> D145N-CA-H 117.706 53.611 7.414 >>D146N-D145CA-D146H 126.659 53.700 9.002 >> D146N-CA-H 126.624 57.133 9.006 >>E147N-D146CA-E147H 118.122 57.097 8.549 >> E147N-CA-H 117.952 58.403 8.548 >>K148N-E147CA-K148H 116.871 58.360 7.998 >> K148N-CA-H 116.895 55.290 7.999 >>S149N-K148CA-S149H 117.591 55.263 7.525 >> S149N-CA-H 117.610 60.926 7.528 >>F150N-S149CA-F150H 127.261 60.881 8.502 >> F150N-CA-H 127.131 57.962 8.495 >>S151N-F150CA-S151H 121.252 58.189 7.960 >> S151N-CA-H 121.264 56.473 7.965 >>R152N-S151CA-R152H 117.847 56.468 9.028 >> R152N-CA-H 117.841 55.064 9.031 >>R153N-R152CA-R153H 120.910 54.972 8.614 >> R153N-CA-H 120.952 55.415 8.616 >>I154N-R153CA-I154H 112.584 55.407 9.128 >> I154N-CA-H 112.595 59.560 9.121 >> H156N-CA-H 122.898 56.435 8.621 >>F159N-F158CA-F159H 121.922 53.507 7.980 >> F159N-CA-H 121.882 55.424 7.976 >>N163N-E162CA-N163H 124.008 57.972 8.745 >> N163N-CA-H 123.940 55.461 8.736 >> F167N-CA-H 118.745 54.370 7.749 >>M171N-F170CA-M171H 111.214 59.121 7.467 >> M171N-CA-H 111.188 55.043 7.464 >>A172N-M171CA-A172H 126.150 55.149 9.030 >> A172N-CA-H 126.033 53.558 9.030 >>W173N-A172CA-W173H 126.926 53.627 9.083 >> W173N-CA-H 126.853 60.803 9.092 >>E175N-S174CA-E175H 120.691 60.569 6.810 >> E175N-CA-H 120.710 58.593 6.809 >>V176N-E175CA-V176H 115.922 58.555 7.231 >> V176N-CA-H 115.927 65.144 7.232 >>T177N-V176CA-T177H 102.542 65.073 7.299 >> T177N-CA-H 102.532 61.772 7.295 >>D178N-T177CA-D178H 123.763 61.726 6.923 >> D178N-CA-H 123.796 52.045 6.926 >>E180N-P179CA-E180H 116.123 65.106 8.555 >> E180N-CA-H 116.151 57.366 8.557 >>K181N-E180CA-K181H 116.535 57.340 7.788 >> K181N-CA-H 116.535 57.340 7.788 >>G182N-K181CA-G182H 104.444 57.349 7.446 >> G182N-CA-H 104.425 46.773 7.445 >>F183N-G182CA-F183H 117.019 46.542 9.069 >> F183N-CA-H 116.943 58.689 9.056 >>I184N-F183CA-I184H 116.317 58.669 7.578 >> I184N-CA-H 116.275 59.163 7.582 >>D185N-I184CA-D185H 126.597 59.200 8.127 >> D185N-CA-H 126.593 53.629 8.129 >>D186N-D185CA-D186H 127.893 53.562 8.954 >> D186N-CA-H 127.939 55.636 8.967 >>D187N-D186CA-D187H 114.529 55.626 8.667 >> D187N-CA-H 114.519 54.742 8.660 >>K188N-D187CA-K188H 115.969 54.953 7.496 >> K188N-CA-H 115.969 54.953 7.496 >>V189N-K188CA-V189H 124.314 54.999 7.897 >> V189N-CA-H 124.315 61.203 7.896 >>T190N-V189CA-T190H 125.410 61.191 10.216 >> T190N-CA-H 125.447 63.424 10.215 >>F191N-T190CA-F191H 126.845 63.331 8.786 >> F191N-CA-H 126.749 56.401 8.791 >>E192N-F191CA-E192H 123.477 56.410 10.009 >> E192N-CA-H 123.472 54.754 10.003 >>V193N-E192CA-V193H 124.593 54.721 8.701 >> V193N-CA-H 124.607 59.978 8.702 >>F194N-V193CA-F194H 126.596 59.940 8.321 >> F194N-CA-H 126.642 55.226 8.319 >>V195N-F194CA-V195H 126.246 55.207 8.822 >> V195N-CA-H 126.235 58.853 8.822 >>Q196N-V195CA-Q196H 124.675 58.901 8.351 >> Q196N-CA-H 124.696 54.616 8.355 >>A197N-Q196CA-A197H 127.932 54.611 8.502 >> A197N-CA-H 127.941 50.676 8.496 >>D198N-A197CA-D198H 126.257 50.644 8.984 >> D198N-CA-H 126.257 53.829 8.981 >>A199N-D198CA-A199H 120.935 53.799 8.465 >> A199N-CA-H 120.928 51.189 8.462 >> H201N-CA-H 118.246 57.326 8.990 >>G202N-H201CA-G202H 104.444 57.349 7.446 >> G202N-CA-H 104.425 46.579 7.448 >>V203N-G202CA-V203H 115.353 46.439 7.561 >> V203N-CA-H 115.382 60.818 7.580 >>A204N-V203CA-A204H 127.421 60.810 8.057 >> A204N-CA-H 127.354 52.283 8.055 >>W205N-A204CA-W205H 125.593 52.305 7.444 >> W205N-CA-H 125.590 58.603 7.444 >>; >> >> loop_ >> _Spectral_dim.ID >> _Spectral_dim.Axis_code >> _Spectral_dim.Spectrometer_frequency >> _Spectral_dim.Atom_type >> _Spectral_dim.Atom_isotope_number >> _Spectral_dim.Spectral_region >> _Spectral_dim.Magnetization_linkage_ID >> _Spectral_dim.Under_sampling_type >> _Spectral_dim.Sweep_width >> _Spectral_dim.Sweep_width_units >> _Spectral_dim.Value_first_point >> _Spectral_dim.Absolute_peak_positions >> _Spectral_dim.Acquisition >> _Spectral_dim.Center_frequency_offset >> _Spectral_dim.Encoding_code >> _Spectral_dim.Encoded_reduced_dimension_ID >> _Spectral_dim.Entry_ID >> _Spectral_dim.Spectral_peak_list_ID >> >> 1 . . H 1 HN . aliased 12019.231 Hz . . . . . . 50080 3 >> 2 . . C 13 C . aliased 12000.000 Hz . . . . . . 50080 3 >> 3 . . N 15 N . aliased 2900.022 Hz . . . . . . 50080 3 >> >> stop_ >> >>save_ >> ; save_ save_spectral_peak_list_4 _Saveframe_category spectral_peak_list _Details '15N/13C USP7 TRAF-like domain HNCO' _Experiment_label '3D HNCO' _Number_of_spectral_dimensions 3 loop_ _Expt_dimension_ID _Atom_type _Spectral_region 1 H HN 2 C C 3 N N stop_ _Sample_label $sample_1 _Sample_conditions_label $sample_conditions_1 _Text_data_format "NMR-STAR v3" _Text_data ; >>save_spectral_peak_list_4 >> _Spectral_peak_list.Sf_category spectral_peak_list >> _Spectral_peak_list.Sf_framecode spectral_peak_list_4 >> _Spectral_peak_list.Entry_ID 50080 >> _Spectral_peak_list.ID 4 >> _Spectral_peak_list.Name . >> _Spectral_peak_list.Sample_ID 1 >> _Spectral_peak_list.Sample_label $sample_1 >> _Spectral_peak_list.Sample_condition_list_ID 1 >> _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 >> _Spectral_peak_list.Chem_shift_reference_ID . >> _Spectral_peak_list.Chem_shift_reference_label . >> _Spectral_peak_list.Experiment_ID 4 >> _Spectral_peak_list.Experiment_name '3D HNCO' >> _Spectral_peak_list.Experiment_class . >> _Spectral_peak_list.Experiment_type . >> _Spectral_peak_list.Number_of_spectral_dimensions 3 >> _Spectral_peak_list.Chemical_shift_list . >> _Spectral_peak_list.Assigned_chem_shift_list_ID . >> _Spectral_peak_list.Assigned_chem_shift_list_label . >> _Spectral_peak_list.Details '15N/13C USP7 TRAF-like domain HNCO' >> _Spectral_peak_list.Text_data_format text >> _Spectral_peak_list.Text_data >>; >>Assignment w1 w2 w3 >> >> R66N-W65C-R66H 121.305 175.457 7.544 >> S67N-R66C-S67H 116.540 174.657 8.836 >> E68N-S67C-E68H 116.241 172.584 7.474 >> A69N-E68C-A69H 119.021 174.742 8.335 >> T70N-A69C-T70H 115.641 175.147 8.266 >> F71N-T70C-F71H 124.642 174.204 9.443 >> Q72N-F71C-Q72H 116.817 172.140 8.565 >> F73N-Q72C-F73H 121.632 175.616 9.509 >> T74N-F73C-T74H 126.858 173.413 8.785 >> V75N-T74C-V75H 129.498 172.679 9.114 >> E76N-V75C-E76H 125.118 174.812 8.105 >> R77N-E76C-R77H 118.982 175.218 8.900 >> F78N-R77C-F78H 121.796 178.734 9.250 >> S79N-F78C-S79H 109.995 177.369 9.533 >> R80N-S79C-R80H 120.613 176.512 7.810 >> L81N-R80C-L81H 124.481 176.271 7.931 >> E83N-S82C-E83H 120.094 173.099 7.690 >> S84N-E83C-S84H 111.735 173.420 8.109 >> V85N-S84C-V85H 120.099 174.646 9.185 >> L86N-V85C-L86H 123.263 173.232 8.087 >> S87N-L86C-S87H 119.261 176.605 8.548 >> C90N-P89C-C90H 123.123 175.345 8.967 >> F91N-C90C-F91H 128.525 174.696 8.967 >> V92N-F91C-V92H 123.395 175.426 8.596 >> R93N-V92C-R93H 124.340 177.126 9.305 >> N94N-R93C-N94H 109.438 173.712 8.727 >> L95N-N94C-L95H 118.691 173.055 7.751 >> W97N-P96C-W97H 126.596 175.461 8.520 >> K98N-W97C-K98H 117.307 175.597 9.206 >> I99N-K98C-I99H 122.405 175.661 8.537 >> M100N-I99C-M100H 128.263 173.441 9.091 >>V101N-M100C-V101H 125.969 174.104 8.669 >>D108N-P107C-D108H 113.379 177.062 8.696 >>R109N-D108C-R109H 118.816 174.172 7.501 >>V115N-S114C-V115H 119.895 172.368 8.965 >>G116N-V115C-G116H 117.868 173.373 9.379 >>F117N-G116C-F117H 127.641 170.565 7.255 >>F118N-F117C-F118H 124.449 172.849 9.734 >>L119N-F118C-L119H 122.883 172.554 9.139 >>Q120N-L119C-Q120H 127.080 174.078 9.745 >>C121N-Q120C-C121H 128.241 174.227 9.434 >>N122N-C121C-N122H 121.899 173.937 8.071 >>A123N-N122C-A123H 118.186 175.859 7.464 >>E124N-A123C-E124H 115.182 178.253 8.169 >>S125N-E124C-S125H 112.493 176.190 6.802 >>D126N-S125C-D126H 125.981 174.001 8.750 >>S127N-D126C-S127H 114.760 176.262 8.263 >>S129N-T128C-S129H 115.636 175.773 8.429 >>W130N-S129C-W130H 120.664 174.138 6.957 >>S131N-W130C-S131H 111.657 175.299 8.947 >>C132N-S131C-C132H 120.996 174.042 9.520 >>H133N-S132C-H133H 133.157 173.356 9.455 >>A134N-H133C-A134H 127.155 173.562 8.600 >>Q135N-A134C-Q135H 117.107 175.150 8.307 >>A136N-Q135C-A136H 122.231 174.291 8.925 >>V137N-A136C-V137H 120.996 175.667 9.099 >>L138N-V137C-L138H 132.073 174.343 9.050 >>K139N-L138C-K139H 125.634 174.242 9.590 >>I140N-K139C-I140H 126.001 175.118 9.083 >>I141N-I140C-I141H 127.105 175.668 7.772 >>N142N-I141C-N142H 126.291 175.148 8.441 >>Y143N-N142C-Y143H 124.746 174.731 8.336 >>R144N-Y143C-R144H 117.178 176.839 7.480 >>D145N-R144C-D145H 117.706 176.885 7.412 >>D146N-D145C-D146H 126.659 176.190 9.009 >>E147N-D146C-E147H 117.966 178.998 8.547 >>K148N-E147C-K148H 116.894 177.812 8.004 >>S149N-K148C-S149H 117.608 177.181 7.527 >>F150N-S149C-F150H 127.119 172.256 8.495 >>S151N-F150C-S151H 121.263 173.776 7.965 >>R152N-S151C-R152H 117.840 172.786 9.030 >>R153N-R152C-R153H 120.941 174.313 8.617 >>I154N-R153C-I154H 112.574 176.607 9.120 >>H156N-S155C-H156H 122.852 175.125 8.614 >>F159N-F158C-F159H 121.899 174.791 7.976 >>N163N-E162C-N163H 123.976 173.417 8.734 >>F167N-G166C-F167H 118.730 176.051 7.739 >>M171N-F170C-M171H 111.145 175.775 7.464 >>A172N-M171C-A172H 126.096 173.912 9.030 >>W173N-A172C-W173H 126.880 178.471 9.097 >>E175N-S174C-E175H 120.702 174.937 6.809 >>V176N-E175C-V176H 115.921 177.033 7.231 >>T177N-V176C-T177H 102.529 176.156 7.294 >>D178N-T177C-D178H 123.798 174.142 6.926 >>E180N-P179C-E180H 116.138 178.453 8.556 >>K181N-E180C-K181H 116.530 178.518 7.788 >>G182N-K181C-G182H 104.419 178.285 7.444 >>F183N-G182C-F183H 116.935 172.253 9.058 >>I184N-F183C-I184H 116.275 173.427 7.582 >>D185N-I184C-D185H 126.580 173.827 8.129 >>D186N-D185C-D186H 127.918 175.708 8.961 >>D187N-D186C-D187H 114.510 175.259 8.662 >>K188N-D187C-K188H 116.017 173.735 7.498 >>V189N-K188C-V189H 124.317 176.341 7.907 >>T190N-V189C-T190H 125.410 174.139 10.214 >>F191N-T190C-F191H 126.845 170.725 8.786 >>E192N-F191C-E192H 123.491 174.380 10.007 >>V193N-E192C-V193H 124.583 173.925 8.701 >>F194N-V193C-F194H 126.673 174.089 8.319 >>V195N-F194C-V195H 126.226 174.258 8.823 >>Q196N-V195C-Q196H 124.746 171.385 8.354 >>A197N-Q196C-A197H 127.946 174.360 8.494 >>D198N-A197C-D198H 126.257 177.256 8.982 >>A199N-D198C-A199H 120.919 174.252 8.463 >>H201N-P200C-H201H 118.232 174.484 9.006 >>G202N-H201C-G202H 104.419 178.285 7.444 >>V203N-G202C-V203H 115.347 174.363 7.578 >>A204N-V203C-A204H 127.397 175.032 8.050 >>W205N-A204C-W205H 125.596 175.851 7.444 >>; >> >> loop_ >> _Spectral_dim.ID >> _Spectral_dim.Axis_code >> _Spectral_dim.Spectrometer_frequency >> _Spectral_dim.Atom_type >> _Spectral_dim.Atom_isotope_number >> _Spectral_dim.Spectral_region >> _Spectral_dim.Magnetization_linkage_ID >> _Spectral_dim.Under_sampling_type >> _Spectral_dim.Sweep_width >> _Spectral_dim.Sweep_width_units >> _Spectral_dim.Value_first_point >> _Spectral_dim.Absolute_peak_positions >> _Spectral_dim.Acquisition >> _Spectral_dim.Center_frequency_offset >> _Spectral_dim.Encoding_code >> _Spectral_dim.Encoded_reduced_dimension_ID >> _Spectral_dim.Entry_ID >> _Spectral_dim.Spectral_peak_list_ID >> >> 1 . . H 1 HN . aliased 12019.231 Hz . . . . . . 50080 4 >> 2 . . C 13 C . aliased 12000.000 Hz . . . . . . 50080 4 >> 3 . . N 15 N . aliased 2900.022 Hz . . . . . . 50080 4 >> >> stop_ >> >>save_ >> ; save_ save_spectral_peak_list_5 _Saveframe_category spectral_peak_list _Details '15N USP7 TRAF-like domain DNA polymerase iota complex' _Experiment_label '2D 1H-15N HSQC' _Number_of_spectral_dimensions 2 loop_ _Expt_dimension_ID _Atom_type _Spectral_region 1 H HN 2 N N stop_ _Sample_label $sample_2 _Sample_conditions_label $sample_conditions_1 _Text_data_format "NMR-STAR v3" _Text_data ; >>save_spectral_peak_list_5 >> _Spectral_peak_list.Sf_category spectral_peak_list >> _Spectral_peak_list.Sf_framecode spectral_peak_list_5 >> _Spectral_peak_list.Entry_ID 50080 >> _Spectral_peak_list.ID 5 >> _Spectral_peak_list.Name . >> _Spectral_peak_list.Sample_ID 2 >> _Spectral_peak_list.Sample_label $sample_2 >> _Spectral_peak_list.Sample_condition_list_ID 1 >> _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 >> _Spectral_peak_list.Chem_shift_reference_ID . >> _Spectral_peak_list.Chem_shift_reference_label . >> _Spectral_peak_list.Experiment_ID 1 >> _Spectral_peak_list.Experiment_name '2D 1H-15N HSQC' >> _Spectral_peak_list.Experiment_class . >> _Spectral_peak_list.Experiment_type . >> _Spectral_peak_list.Number_of_spectral_dimensions 2 >> _Spectral_peak_list.Chemical_shift_list . >> _Spectral_peak_list.Assigned_chem_shift_list_ID . >> _Spectral_peak_list.Assigned_chem_shift_list_label . >> _Spectral_peak_list.Details '15N USP7 TRAF-like domain DNA polymerase iota complex' >> _Spectral_peak_list.Text_data_format text >> _Spectral_peak_list.Text_data >>; >>R66N-H 121.508 7.558 >> S67N-H 116.547 8.840 >> E68N-H 116.404 7.475 >> A69N-H 119.115 8.348 >> T70N-H 115.737 8.266 >> F71N-H 124.803 9.442 >> Q72N-H 116.899 8.566 >> F73N-H 121.694 9.507 >> T74N-H 126.959 8.779 >> V75N-H 129.594 9.116 >> E76N-H 125.184 8.121 >> R77N-H 119.074 8.901 >> F78N-H 121.871 9.253 >> S79N-H 109.990 9.522 >> R80N-H 120.664 7.796 >> L81N-H 124.635 7.939 >> E83N-H 120.133 7.687 >> S84N-H 111.751 8.102 >> V85N-H 120.173 9.176 >> L86N-H 123.305 8.092 >> S87N-H 119.343 8.542 >> C90N-H 123.294 8.989 >> F91N-H 128.589 8.977 >> V92N-H 123.511 8.557 >> R93N-H 124.390 9.299 >> N94N-H 109.647 8.703 >> L95N-H 118.645 7.744 >> W97N-H 127.197 8.507 >> K98N-H 117.341 9.199 >> I99N-H 122.672 8.529 >> M100N-H 128.499 9.131 >> V101N-H 125.966 8.663 >> M102N-H 121.007 8.624 >> D108N-H 113.290 8.716 >> R109N-H 118.903 7.512 >> V115N-H 119.906 8.971 >> G116N-H 117.917 9.384 >> F117N-H 127.624 7.155 >> F118N-H 124.157 9.724 >> L119N-H 123.190 9.125 >> Q120N-H 127.450 9.833 >> C121N-H 128.538 9.530 >> N122N-H 122.021 8.079 >> A123N-H 118.521 7.470 >> E124N-H 115.187 8.162 >> S125N-H 112.553 6.796 >> D126N-H 126.137 8.749 >> S127N-H 114.808 8.243 >> S129N-H 115.267 8.395 >> W130N-H 120.746 6.948 >> S131N-H 111.776 8.994 >> C132N-H 120.960 9.434 >> H133N-H 133.398 9.466 >> A134N-H 127.197 8.507 >> Q135N-H 117.220 8.316 >> A136N-H 122.158 8.916 >> V137N-H 121.009 9.094 >> L138N-H 131.749 9.026 >> K139N-H 125.662 9.594 >> I140N-H 126.072 9.093 >> I141N-H 127.178 7.777 >> N142N-H 126.398 8.427 >> Y143N-H 124.822 8.342 >> R144N-H 117.335 7.478 >> D145N-H 117.772 7.412 >> D146N-H 126.411 9.011 >> E147N-H 118.046 8.543 >> K148N-H 116.989 8.004 >> S149N-H 117.700 7.525 >> F150N-H 127.197 8.507 >> S151N-H 121.363 7.953 >> R152N-H 117.566 9.026 >> R153N-H 121.007 8.624 >> I154N-H 112.281 9.141 >> H156N-H 122.846 8.598 >> L157N-H 117.993 6.172 >> F159N-H 121.669 8.002 >> H160N-H 122.297 8.036 >> N163N-H 123.709 8.728 >> F167N-H 118.654 7.722 >> N169N-H 117.188 7.301 >> F170N-H 119.129 8.693 >> M171N-H 111.284 7.456 >> A172N-H 126.411 9.011 >> W173N-H 127.049 9.092 >> E175N-H 120.803 6.802 >> V176N-H 116.019 7.232 >> T177N-H 102.644 7.284 >> D178N-H 123.921 6.929 >> E180N-H 116.199 8.553 >> K181N-H 116.645 7.784 >> G182N-H 104.452 7.449 >> F183N-H 116.987 9.055 >> I184N-H 116.405 7.579 >> D185N-H 126.693 8.144 >> D186N-H 128.250 8.975 >> D187N-H 114.613 8.661 >> K188N-H 116.066 7.497 >> V189N-H 124.319 7.896 >> T190N-H 125.454 10.197 >> F191N-H 126.959 8.779 >> E192N-H 123.532 10.012 >> V193N-H 124.648 8.701 >> F194N-H 126.731 8.289 >> V195N-H 126.254 8.826 >> Q196N-H 124.822 8.342 >> A197N-H 128.002 8.506 >> D198N-H 126.411 9.011 >> A199N-H 120.823 8.464 >> H201N-H 118.181 9.017 >> G202N-H 104.452 7.449 >> V203N-H 115.245 7.556 >> A204N-H 127.491 8.052 >> W205N-H 125.714 7.446 >>; >> >> loop_ >> _Spectral_dim.ID >> _Spectral_dim.Axis_code >> _Spectral_dim.Spectrometer_frequency >> _Spectral_dim.Atom_type >> _Spectral_dim.Atom_isotope_number >> _Spectral_dim.Spectral_region >> _Spectral_dim.Magnetization_linkage_ID >> _Spectral_dim.Under_sampling_type >> _Spectral_dim.Sweep_width >> _Spectral_dim.Sweep_width_units >> _Spectral_dim.Value_first_point >> _Spectral_dim.Absolute_peak_positions >> _Spectral_dim.Acquisition >> _Spectral_dim.Center_frequency_offset >> _Spectral_dim.Encoding_code >> _Spectral_dim.Encoded_reduced_dimension_ID >> _Spectral_dim.Entry_ID >> _Spectral_dim.Spectral_peak_list_ID >> >> 1 . . H 1 HN . aliased 8012.821 Hz . . . . . . 50080 5 >> 2 . . N 15 N . aliased 1400.000 Hz . . . . . . 50080 5 >> >> stop_ >> >>save_ >> ; save_